TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Pentacosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

15.17 0.30 ug/1 59279 Naphthalene-d8 15.87 Hit# of/ 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 59 2 Tetradecane 198 C14H30 000629-59-4 59 3 Docosane 310 C22H46 000629-97-0 59 4 Eicosane 282 C20H42 000112-95-8 59 Abundance Scan 1103 (15.169 min): 8481.D (-) m/ z 43.05 100.00% 43 57 71

5000

— 85

99 127 ' "I I I ■ I

14.80 15.00 15.20 15.40 I I I-1 > I U_s I I I I I I I I I I I I

r 11 ’ I — 1 i II.. II............ . n i i । । । i i । i—। "ti । i । i i Iu । i । । । i । [ i । । । । । । 1 i । n । । । । r m/z 57.00 99.17% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73718: Pentacosane / 43 57

5000 71 1+7*1 1 1* 1‘’1 11‘‘IUUIIIU V 85 14.80 15.00 15.20 15.40 m/z 70.95 68.94% 99 .

m/z-> 20 ...40l 1 1 60| JL80li 100 iJ 113127141 155169183197211225 ।1 ■ ■ ■ । 120 140 160 180 200 220 240 260 280 300 Abundance 43 57

71 #69661: Tetradecane AA J W U 1 I >■ "TT J I I 1 ' I 1 ' ' ' 1 1 ' ' 1 1 1 14.80 15.00 15.20 15.40 5000 m/ z 41.05 58.73% 85

27 ,

m/z-> Abundance 20 I. 40 43 57 V’ 60 99 113 - 155 i ‘ 1 1 1 i 198 | । । । । | i i । । | 1 । > । | r

80 100 120 140 160 180 200 220 240 260 280 300 #72997: Docosane ( i । i i i i । i i I‘07

NNU।. । । i । । । 14.80 15.00 15.20 15.40 iiii AAN । > > । । । । । । । । ।

m/z 85.05 41.13% 71 5000 85

i ■ ■ ■ > ।1 J ...... 1 — 1 r11n99l ' 113127 155169183197211 292 310 AA N U _ A A 1 1 1 i ' ' ' i ' 1 11 1 ' 1 1 ' i 1 1 1 1 1 1 '1 1 I ri 1 1 I । ' ' 'I ri'' । । ' 1 1 1 1 1 1 1 1 ' 1 ’ ' I ' 1 ' '■ I'1 1 1 1 1-1111 I > mfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 14.80 15.00 15.20 15.40

8481.D GCMS0412.M Fri Apr 26 12:47:26 2002 Page 7

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