GCMS analysis results for sample AE10807, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0802\10807.D Vial: 22 Acq On 9 May 2002 7:08 am Operator: Sample GC/MS SCAN 5/7 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************** * ********** Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 17.95 0.90 ug/1 67076 Naphthalene-d8 15.83

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexa loxane, dodecamethyl- 444 C12H3606Si6 000540-97- . 2 Silane, [ ,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2-9- 3 2H-1,4-Renzodiazepin-2-one , 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 4 1,1,1,5/7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 9 Abundance Scan 1409 (17.954 min): 10807.D (-) m/ z 73.10 100.00% 73 1 5000 341 ................... I I I (........................ I I I I I I I I I I I I I I I I I 1 I T 147 429 45 17.60 17.80 18.00 18.20 I 117 [ 207 251 L I 10011181 ।"1 'i ■ l ‘■ I TTE——311 TT mRgT m/ Z 341.00 37.86% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341

429 5000 1 1 i 1 1 1 ■ i ■ ■ i 1 1 1 ' i 1 17.60 17.80 18.00 18.20 147 m/z 147.05 14.07% 117 | 207 267 311 [ ......... ■ ■ i | ' i i i | i I i i | i r i I | I I I ITTT77 I I I I | M" I | n II | ir"11 r1" i I I I I I I I I I I I 1 I I I I I I I I I ~| Ti i i | i l i t । i

m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 73 TrII 11 'i 11 TIBOTETGTT 239 17.60 17.80 18.00 18.20 5000 342 m/z 429.05 13.28%

45 | 133, 179 211 314 1 i i ■ | i i i i | i i > ■ | > > i r | i i i i | ( Fl i । i T I i | i i i i | i i ■ i | i i i i | i i i i "I ""I" "I ""i'1 "I m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 17 73 341 17.60 17.80 18.00 18.20 m/z 342.00 12.24%

5000 45 | 116 146 t i i । i I i i J| i i i i । i i i i । i r i * I | i i r t । i i i i । TmnTnTTTT^nTrr^^ 227 269 315 _____________ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.60 17.80 18.00 18.20

10807.D GCMS0507.M Fri May 10 08:21:09 2002 Page 3

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