Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
NYC-WTC_000039497–000039521Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR1702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.
17.97 2.00 ug/1 326690 Naphthal ene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 Silane, [1,2,3/-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 12 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 10 4 Trimethylsily [3-methoxy-4-(trimet 326 C15H26O4Si2 037148-61-1 9 Abundance 1 Scan 1407 (17.965 min): 6449.D (-) m/z 73.00 100.00% 73
5000 341
147 429 ' I ' 1 1 ' I 1 1 r 1 f ‘ ' 1 I • ‘ ' I T 17.60 17.80 18.00 18.20
m/z—> 45 - 117 TUT I, rff' n 179 - 207
40 60 80 100120140160180200220240260280300320340360380400420 251 281 311 [ TTTTT 397.4 m/z 341.00 49.21% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 "I 17 17.60 17.80 18.00 18.20 147 m/z 147.00 17.03% T‘‘‘101‘111 117 | 11"11"1111 ’" I" " I 207 i'■ i 267 i'111 in 111 311 | 1’11117 T 1’11111011110111111111 I miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 73 239 TT A Tlt 1 i 1 ■ 1 1 i 1 17.60 17.80 18.00 18.20 342 5000 m/z 342.00 16.10%
45 133 211 —....... TT - p-rrrp-rrrj- I1 ’" 1"" 111 "I ""I ! I I I | I I H | 1 I I I | r 111 r m/z-> Abundance 40 60 80 100120140160180 200 220 240 260 2^)300 320 340 360 380 400 420 #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- ........ L ■ 1 i 1 ' ■ ■ i ' 73 341 17.60 17.80 18.00 18.20 m/z 429.15 15.87% 5000 45
I I 227269 116 146 TTTTT TTTTT] I" "I''"I ”1111" I" " I ’11' 1111111 315, .................. /.................... 1 1 ' 1 1 1 1 1 1 ' 1 I1 1 1 1 I 1 1 1 1 1 1 m/z—> 40 60 80 100120140160180200220240260280300 320340360380400420 17.60 17.80 18.00 18.20
6449.D GCMS0412.M ThU Apr 18 09:10:46 2002 Page 4
NYC-WTC_000039507
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NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039545
Laboratory report documenting GCMS analysis of sample AE06452 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder