Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
NYC-WTC_000039469–000039496Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.97 3.12 ug/1 503633 Naphthalene-d8 15.85
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 42 2 Acetic acid, /[bis [ (trimethylsilyl) o 356 CllH29O5PSi3 053044-27-2 42 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, [1,2 benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 14 Abundance » Scan 1408 (17.968 min): 6430.D (-) m/ z 73.00 100.00% 73
341 5000
147 429 .......... ' i 1 1 ‘ J.............. ‘ 1 r ‘ i 1 1 1 i ■ i 1 1 1 1 1 1 i 45 17.60 17.80 18.00 18.20 117 179,. 207 251 281 311 | 397 1’i11’1। 1’111111111 TTTT I TUTT TT TTTT I I / j I IT TT 1 * [ 1 1 TTT TTT 1 1 I TTT 1I‘ m/z 341.00 52.99% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
5000 429 .......... H............ 1 । ' ' ' 1 । ' TT । । । । i i i । । । 17.60 17.80 18.00 18.20 147 m/z 429.05 18.15% 117 ! 207 "' r 11' i" " ।1 ■ ■ > । " T’ "‘I’'' TTTT , 11111114 [ 11 267 TCTTOgu TTTT 311 [ mlz—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #49839: Acetic acid, [bis[(trimethylsilyl)oxy]phosphinyl]-, 73 341 . .......... -----........... 17.60 17.80 18.00 18.20 5000 m/z 147.00 17.81%| 251 297
m/z— > . . I mH 133 1" i1" 1 r ■ " i" “ i" ■1111111 ‘"11 211
40 60 80 100120140160180200220240260280300320340360380400420 TH AH i ‘ 111111111—001—1311131107
Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.60 17.80 18.00 18.20 m/z 342.00 17.38%| 5000 45
.16 146... 227. 269. 315/_ 1 ■' I" '11" '' 111 " 11 " ' I' ‘ ‘ ■ l'' " I' • ‘' I'''' I'1 " I' " 11' " 11' ‘' I " '' I''' ‘ I'1 "T1" 11"1111111111111111111 ‘ । 1 1 1 > । * 1 । 1 >> < । । । । ' । । m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 17.60 17.80 18.00 18.20
6430.D GCMS0412.M Thu Apr 18 09:09:23 2002 Page 6
NYC-WTC_000039481
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
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NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
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Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
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NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder