Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
NYC-WTC_000039469–000039496Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Imidazole-4-carboxamide Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 18.68 0.75 ug/1 133625 Acenaphthene-dl0 21.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Imidazole-4-carboxamide ill C4H5N3O 000000-00-0 23 2 Cyclohexane, 1,4-dimethyl-2-octadec 364 C26H52 055282-02-5 12 3 2 (1H) -Pyrimidinone, 4-amino- 111 C4H5N3O 000071-30-7 10 4 3,4-Dimebhylthiophene________________ 112 C6H8S 000000-00-0 10 Abundance t Scan 1486 (18.684 min): 6430 dX) m/ z 43.05 100.00%| 43 73 111
5000 95 — .... 18,40 18.60 1 80 19.00
m/z-> 40 —l+l Mn. 60 । 127 146 1111 1 1 '1 h 11T i1' " i " ' ■ i TTT 1111111'1111111111 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 201 T''' 'l'111 l r" 11 ’1 ’' 11'111'1 m/ Z 57.00 78 .98% Abundance #2400: Imidazole-4-carboxamide 1 1 44 68 95 5000 18,40 18.60 18.80 19.00 m/ z 73.00 74.07% ‘'11 t ' ' I ' ' 11 | 1 1" 1 | 1 1 1 1 | 1 1 1 ‘ | ‘ 1 ‘ ‘ | TTT] rn i | i i i | | i , i i | m i । । i i 111 " I ।1 “11" m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #50819: Cyclohexane, 1,4-dimethyl-2-octadecyl- 1 1 ' 1 | 1 ' ■ ■ | i , I r n | | T 1 18.40 18.60 1880 19.00 5000 69 m/z 111.10 69.22%.
m/z-> 40 60 1195 + 323 346 364 | • । • • | ••< । | । 1 • i | < । I I ] I । | | | | | I r | I I I I | I r I I | I I I I | | I | I | | I | | [ | | |
80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #63896: 2(1 H)-Pyrimidinone, 4-amino- .......... _ 1 1 18.40 18.60 18.80 19.00 m/z 95.00 37.22% 5000
69 42
m/z-> IX40 95.. 7 j Ut i i | i i i i | I I I r | i i r 1 [ 1 1 1 1 j 1 >1 I [ t 1 I I I I I I I I I I I I I I I I I I I t I I I I I I I I I I I I I I I I 1 I I I I I I I I
60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 —... — i 1 ‘ ' 1 i ' ' 18.40 18.60 18.80 19.00
6430.D GCMS0412.M Thu Apr 18 09:09:24 2002 Page 7
NYC-WTC_000039482
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder