GCMS analysis results for sample AE06449, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\APR1702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 Imidazole-4-carboxamide Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 18.68 0.81 ug/1 148897 Acenaphthene-dl0 21.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Imidazole-4-carboxamide 111 C4H5N3O 000000-00-0 23 2 Thiophene, 2, 5 - dimethyl - 112 C6H8S 000638-02-8 16 3 Propanenitrile, 3-(ethylpropylamino 140 C8H16N2 055619-10-8 12 4 Cyclohexane/ 1,4-dimethyl-2-octadec 364 C26H52 055282-02-5 12 Abundance » Scan 1485 (18.681 min): 6449.D (-) m/z 43.00 100.00% 43 57 73 111 5000 95 ......

mlz—> TT 4 I r++++83 TTTT i'11' i , 127 146 201 1' 11111111' TTTTT TICTTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Im. * m/z 18.40 18.60 18.80 19.00 57.00 74.09% Abundance #2400: lmidazole-4-carboxamide 1 1 44 68 95 5000 18.40 18.60 18.80 19.00 m/z 73.00 72.21%

mlz-> 11111' i m 53 83 i ■ ■ ■ ■ i ■ 11 ■ i ■ i«■ i1 > ■ ■ [ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #63946: Thiophene, 2,5-dimethyl- 1 1 1 ■ i ■ ■ 18.40 18.60 18.80 19.00 5000 97 m/z 111.10 59.99%

45 59 | 169 78 Pm TT TTT i " 111 I— 11 “ 11' " 11 “ 1' I 111112’1—1111 mz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #7431: Propanenitrile, 3-(ethylpropylamino)- ■ 1 i ■ 1 1 ■ i ■ 1 1 ' i ‘ ‘ i ' ■ 1 1 18.40 18.60 18.80 19.00 m/z 95.00 37.05% 100 5000

83 42 58 | ,.| .. I,...... 125 140 _ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 18.40 18.60 18.80 19.00

6449.D GCMS0412.M Thu Apr 18 09:10:47 2002 Page 5

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