Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
NYC-WTC_000039588–000039610Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\6455.D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 7 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T. 20.80 1.25 ug/1 202526 Acenaphthene-dl0 21.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy/l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 10 4 Silane, [bicyclo [4.2.0]octa-3,7-die 282 C14H2602Si2 036461-33-3 9 t Scan 1716 (20.796 min): 6455.D (-) Abundance m/z 73.00 100.00% 73
5000 147 281
327 I 1 1 1 1 I ' 1 P —A 45I [ 191 221 249 20.40 20.60 20.80 21.00 21.20 1 1 1 1 1 117 , — I — + 1 —— L L 383 415 .... . , m/ z 2 81.00 45.15% mlz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 20.40 20.60 20.80 21.00 21.20 m/Z 147.00 43.09% 221 281 327 ----------------- 1 415 519 561 ' 1 1 1 1 1 1 i ' 1 1 1 1 1 " 1 ' i ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 -|-r-r-r-i-|—r-r I11 1 1 i 1 281 20.40 20.60 20.80 21.00 21.20 5000 m/z 326.90 16.34%
369
■ • i ■ ■ ■ • i ■ 207 249 ------------I- 13 mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317: 4-Amino-5-imidazole carboxamide, tris(trimethylsily - 73 20.40 20.60 20.80 21.00 21.20 m/z 282.00 11.95% 327 5000 237 45 147
m/z-> 50 ...... 172 212 100 150 200 4 250 300 350 400 450 500 550 T CIEET 1 'I 1 1 * 1 i 11 20.40 20.60 20.80 21.00 21.20
6455.D GCMS0412.M Thu Apr 18 09:14:18 2002 Page 7
NYC-WTC_000039601
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039574
Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder