Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
NYC-WTC_000039588–000039610Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\6455.D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Thiophene, 2,5-dimethyl- Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
18.68 0.73 ug/1 117263 Acenaphthene-dl0 21.15
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Thiophene, 2,5-dimethyl- 112 C6H8S 000638-02-8 12 2 Hexanal, 5,5-dimethyl- 128 C8H160 055320-58-6 10 3 2 (1H) -Pyrimidinone, 4-amino- 111 C4H5N3O 000071-30-7 9 4 2-Propenenitrile, 3 - (acetyl oxy) - 111 C5H5NO2 014268-54-3 9 Abundance Scan 1486 (18.685 min): 6455. D (-) m/ z 42.95 100.00% 43 57 73 111
5000 95 Ttnap TTTT ———— 18.40 18.60 18.80 19.00 146 1 । 1 1 1 1 । 1 1 1 ■ [ । 49. — H—TT 85 T TT ' 1 i 1 ' 1 1 i -- 127 r1i 1 m/ Z 57.00 73.69% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 1401 150 Abundance #2528: Thiophene, 2,5-dimethyl- 1' 1
97 5000 18.40 18.60 18.80 19.00 45 59 m/ z 73.00 69.30% 27 1434 | ■ I ■ ■ ■ ' i ■ 1 ' ‘ i ' 85 1 i ' 4 TII 1— m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #5025: Hexanal, 5,5-dimethyl- 57 18.40 18.60 18.80 19.00 5000 41 m/z 111.10 66.03% 69 95
84 m/z-> - 20 30 40 50 60 70 + 80 90 100 110 120 130 140 150 Abundance ;#63896: 2(1 H)-Pyrimidinone, 4-amino- ' 1 l 1 1 1 ' i ' 1 1 1 18.40 18.60 18.80 19.00 m/ Z 69.00 35.31%
5000
69
m/z-> 42 55 1 i 1 1 1 1 । 1 1 1 1 । 1 11 TOT ‘ l “ 20 30 40 50 60 70 83 1t |I 95 —TEOTTT +IIPP 80 90 100 110 120 130 140 150 ' 1 i 1 ' ' 1 1 1 18.40 18.60 18.80 19.00
6455.D GCMS0412.M Thu Apr 18 09:14:17 2002 Page 6
NYC-WTC_000039600
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039574
Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder