Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
NYC-WTC_000039588–000039610Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C : \HPCHEM\ 1 \DATA\APR1 702\6455.D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.97 1.82 ug/1 266335 Naphthalene-d8 15.85
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 59 2 Acetic acid, is[(trimethylsilyl)o 356 CllH29O5PSi3 053044-27-2 40 3 2-Chloro-4-(4Amethoxyphenyl)-6-(4-n 341 C17H12C1N3O3 063673-76-7 17 4 1,3,5,7,9-Pentaethylcyclopentasilox 370 C10H30Q5Si5 017995-44-7 13 Abundance Scan 1408 (17.969 min): 6455.D (-) m/ z 73.00 100.00% 73
341 5000
147 429 ‘I I T I" 45 179207 251 281 311 [ 17.60 17.80 18.00 1 8.20
m/z—> TI I'11 'i 117 .. TI—01—0"TETTET[T1TOUTETIETTTT m/z 341.00 40 60 80 100120140160180200220240260280300320340360380400420 58.37% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 / 5000 ■ । 1 1 । ■ j ■ ■ ' 1 i 1 ■ ■ ■ i 1 17.60 17.80 18.00 18.20 147 m/z 429.05 19.64% , 117 | 207 267 311 [ . >. । . 111 > i r. । > 11 > 111.1111111. h। CTTCT i11111 r 1111"111111'r • > < । ■ i • • * ■ । i 11 1 i । mlz—> 40 60 80 100120140160180200220240 260280300320340360380400420 Abundance #49839: Acetic acid, [bis[(trimethylsilyl)oxy]phosphinyl]-, 73 341 \........................ 1 i ' 1 ' 1 I 1 ( 1 ' I ‘ ' 1 1 17.60 17.80 18.00 18.20 5000 m/z 342.00 18.90% 251 297 A 133 211
1111' I"1111" 11 Il l........... LL THTTTT I11'1 r1" I’TETTTT—0011110T mz->__ 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48253:2-Chloro-4-(4-methoxyphenyl)-6-(4-nitrophenyl)pyrim "T TT 341 17.60 17.80 18.00 18.20 m/z 147.00 17.60% 5000
252 295 233 1 276 L TTTWTTTTTTTTTT r "' i"1' i" " i r“ "T" "I 1’111111111171 I" ,rl ”111 m/z—> 40 60 80 100120140160180200220240 260280300320340360380400420 17.60 17.80 18.00 18.20
6455.D GCMS0412.M Thu Apr 18 09:14:16 2002 Page 5
NYC-WTC_000039599
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039574
Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder