NYC-WTC_000038521
Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.
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machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis results for sample AE02577, March 2002
Machine-extracted title · confidence 90%Laboratory report documenting GCMS analysis of sample AE02577 conducted on March 25, 2002, identifying other unknown compounds.
NYC-WTC_000038848–000038860Folder label: “GCMS X 3/4/02 A 3/20/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR1902\2577.D Vial: 26 Acq On : 21 Mar 2002 5:39 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
18.03 0.47 ug/1 78594 Naphthalene-d8 15.91
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane/ dodecamethyl- 444 C12H3606Si6 000540-97-6 40 2 Acetic acid, [bis[(trimethylsilyl )o 356 CllH29O5PSi3 053044-27-2 33 3 1,3,5,7,9-Pentaethylcyclopentasilox 370 C10H3005Si5 017995-44-7 17 4 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 14 Abundance............ ......... “ Scan 1414 (18.027 min): 2577.D () m/ z 73. 00 100.00% 73
341 5000
147 429 1........ 4....... — H 45 i "117 179 207 TIPg T—mg TUIUUTTTH[ 251 311.1. .. I m/z 341.00 '1' i11 ‘11111'1111111 17.60 17.80 18.00 18.20 18.40 55.23% m/z-2 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380400 420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.60 17.80 18.00 18.20 18.40__ 147 m/z 147.00 19.53% 117 1 207 TVTTTTTTTTTTTTTTTTTITTTTT 267 311 '11 ’1111'111 U "11'11'11 TTOO m/z-.. 40_ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance s— ' : olie noid.stmmppem—aannkas.. .. a 73 341 /I 17.60 17.80 18.00 18.20 18.40 5000 297 m/z 342.00 18.75% 251 133 211
m/z-> 40 60 80 100120140160180 200 220240 260 280 300 320 340 360 380 400 420 Abundance #51267:1.3,5.7,9-Pentaethylcyciopentasiloxane ..... , 341 17.60 17.80 18.00 18.20 18.40 m/z 429.05 16.98% 87 5000 59 253 281 197 225 311 . ....m +I I- -369 — 111’ ......... / ........ m/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 17.60 17.80 18.00 18.20 18.40
2577.D GCMS0308.M Thu Mar 21 14:26:42 2002 Page 3
NYC-WTC_000038857
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