GCMS analysis results for sample AE06453, April 2002

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Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039560–000039573

Folder label: “GCMS X 3/19/02 A 4/17/02”

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Data File : C:\HPCHEM\1\DATA\APR1702\6453 .D Vial: 11 Acq On : 17 Apr 2002 6:00 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 17.97 0.51 ug/1 72979 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 Acetic acid,/ [bis[(trimethylsilyl)o 356 CllH29O5PSi3 053044-27-2 38 3 1,3,5,7,9-Pentaethylcyclopentasilox 370 C10H3005Si5 017995-44-7 32 4 2-Chloro-4-/(4-methoxyphenyl)-6-(4-n 341 C17H12C1N3O3 063673-76-7 16 Abundance Scan 1408 (17.970 min): 6453.D (-) m/z 73.00 100.00% 73

341 5000

147 429 45 17.60 17.80 18.00 18.20 1 40 .... i... t " lll"l TT TUTmT 207 1111' 11 •1' I 251 i"'" i‘'"‘I 311.1.. I"" i'"'i'"'i1 1" 11 “111 *" 1111111 m/z 341.00 54.86% mlz->____ 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341

429 5000 [ 1 i ' ' • 1 i • 17.60 17.80 18.00 18.20 18.40 147 m/z 429.15 20.79%| 117 [ 207 267 " i"111"11 r1111' i • i । । । t 11 11 t । । । i t 11 i i i । 11 i 11 ] 11 । 11 i j i i j t 'i r r j 311 L i" " ।"1' i1 ■" i ........... _ TTTIEEIUTTT m/z—> 40 60 80 100120140160180200220240260280300320340360380 400 420 Abundance #49839: Acetic acid, [bis[(trimethylsilyl)oxy]phosphinyl]-, 73 341 ■i ■''■। 11' 1i1' 1 1 i 1 1 1 1 i 1 17.60 17.80 1 8.00 18.20 18.40 5000 m/z 342.00 18.881 251 297 A 133 211 r ‘" i" " i " ‘' i ■'" I' 1 i''111'1' ■ i'1 ■111"11 ■ ■111 ■"11 111'1111 i‘ri ■ ।। । >j। m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #51267:1,3,5,7,9-Pentaethylcyclopentasiloxane 1 TT r TIT 341 17.60 17.80 18.00 18.20 1 40 m/z 147.00 16.99%| 87 5000 59 253 281 197 225 i"'11'i1 •” i' ’" i111 '111111111 'I 1 ’17 i11" r "1 1 -369 311 i""i r - 11 1 1 ■ ‘ I ■ m/z—> 40 60 80 100120140180180200220240260280300320340360380400420 17.60 17.80 18.00 18.20 18.40

6453.D GCMS0412.M Thu Apr 18 09:12:52 2002 Page 4

NYC-WTC_000039570

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GCMS analysis results for sample AE06454, April 2002 · Box DEP Box 23

NYC-WTC_000039574

Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.

1 shared topics · Same agency, volume and box · similarity 0.998