NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AE02645, Mar 15, 2002
Machine-extracted title · confidence 90%Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
NYC-WTC_000005415–000005434Folder label: “GCMS X 2/5/02 A 3/7/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAR0702\2645.D vial: 18 Acq On 8 Mar 2002 6:27 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
18.05 1.40 ug/1 243422 Naphthalene-d8 15.94
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane/ dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 18 3 1,1,1,5,7,7,7- eptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 16 4 2H-1,4-Benzodi, zepin-2-one, 7-chlor 342 C18H19ClN2OSi 73.00 055299-24-6 100.00% 14 Abundance 73 Scan 1417 (18.053 min): 2645.D ().. " [ m/z
5000 341
147 429 I /A..... ......18.00 .17.80 18.20 18.40 45 , , 117 [ 179 207 251 281 311 [ | m/z-> I 1I—001——0I0—0010——0100—0—1———1——011001011—0071—01100—09——0u)7T ’11" 1 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380400 420 . .. np ' m/z 341.00 41.93% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 ....... ............ 5000 17.80 18.00 18.20 18.40 147 m/z 147.00 16.93% 117 207 267 311 " i" " i1 ‘ “ i"'' i"' ■ i ‘"11 ■1'' i1 ‘" i" " i1" ‘ i i" " i" " i" " r " ■ r1'" ■ i11111"111"'1 r11111" ■ i' m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400420 Abundance - ■a • 1 73 239 / \.... 17.80 18.00 18.20 18.40 342 5000 m/z 342.00 14.91% 45 133 211 m/z-> 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380400 420 Abundance #56714: 1.1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethyIsiloxy)t \ 11 TTT 73 17.80 18.00 18.20 18.40 m/ z 325.00 13.59% 147 5000 267 355 429
m/z-> 45 r ■'. i i" " r "' i" " r ’ ■ ■ i 207
111111 r "11''" i' ‘" i ‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 1" " 1"'11" " 1 •'" 1" " 1 ■"' 1' . n.. 17.80 18.00 18.20 18.40
2645.D GCMS0208.M Wed Mar 13 14:54:12 2002 Page 3
NYC-WTC_000005424
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