GC/MS analysis results, sample AE08934, May 2002

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Data File C:\HPCHEM\1\DATA\MAY0302\8934.D Vial: 8 Acq On 3 May 2002 8:54 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 13.41 ug/1 843733 1,4-Dichlorobenzene-d4 12.19

Hit# of Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C(0)OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 341 (8.162 min): 8934.D (-) m/ z 43.05 100.00% 43

5000 59

1 ' I ' ■ 101 7.80 8.00 8.20 8.40 8.60

m/z-> 10 i ■ ■ ■ 1 i ■ 1 20 ■ 1 30 3? | i 1 ■ ■ 1 r■ 40 50 +53 4 60 70 69 80 ■ i ■ 1 ' 83 1 i ' '' 1 1 i ■ ' 1 90 , | 1 i 1 1 100 ' ‘ i ' 110 m/ z 59.10 41.53% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ‘ I’" ' ' I ' ' ' 1 I 1 ’ 1 1 I ' 59 7.80 8.00 8.20 8.40 8.60 m/ z 58.10 16.72% 27 I no 101 — ----- 49—+ I 83 | m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 12.88%

5 |8 72 ............................ .. , 38 100 1 I* m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone i । | > I n | i “i i i । I I T 'I | I I I I | I 43 780 8.00 8.20 8.40 8.60 m/z 41.00 7.03%

5000 15 58 27 ----- Tin T T I 1 ' 1 1 i 1 ' ' 1 i ■ ‘ 1 1 i 1 ' 1 1 i ■ ' 1 ' i ‘ TTTpPuummaopr m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

8934.D GCMS0501.M Mon May 06 10:49:02 2002 Page 1

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