GCMS analysis results for sample AE01462, Feb 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\1462.D Vial: 15 Acq On : 22 Feb 2002 3:53 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Squalane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

24.10 0.24 ug/1 30369 Phenanthrene-dl0 25.74

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Squalane 422 C30H62 000111-01-3 90 2 Hexadecane, 2,6,11,15-tetramethyl- 282 C20H42 000504-44-9 86 3 Pentadecane, 2,6,10,14-tetramethyl- 268 C19H40 001921-70-6 83 4 Dodecane, 2,6,11-trimethyl- 212 C15H32 031295-56-4 64 Abundance. . .. .. Scan 2076 (24.104 min): 1462.D (-) m/z 5 7 ,00 100.00% 57

5000 85 113 183 J._. 23.80 24.00 24.20 24.40 mmmmmmmmmmmmmmmmmmmmmm m/ Z 71 00 85.11% miz-X.... 40 60 80 100 120 140 160 180 200 220 240260280 300 320 340 360 380 400 420 Abundance #74379: Squalane 57

5000 85 404422 ’ ■ T AV 23.80 24.00 24.20 24.40 I 113 m/ Z 43 05 68.38% 141 183 266 337 | 1,11" i" " i" " 11 ‘" i" " i ■"' i TUIugtugu—TT[TT m/z-?......40 6080 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance : 57 -

23.80 24.00 24.20 24.40 5000 m/z 41. 05 34.45% 85 113 169 141 196 '" i " " i" " i" " i1"11" " I'"111 (111111111 r"'i‘ ' i'" ‘ V 111" " 11" ' i1 r'11" " 1111111" 111" Wz-> 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #71951: Pentadecane, 2.6,10,14-tetramethyl- , 4* Ar A ----- 57 23.80 24.00 24.20 24.40 m/z 85 00 31.54% 5000 85 113 .......... । 155 183 238 268 - ‘‘‘111070711-p— "I——1EE—0—U"ET1T111"00101 —Tgtt m/z-> 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 400 420 23.80 24.00 24.20 24.40

1462.D GCMS0308.M Mon Mar 25 08:27:38 2002 Page 6

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