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GCMS analysis results for sample AD31466, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31466 conducted on February 11, 2002.

NYC-WTC_000018405–000018415

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018414
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN1602\31466.D Vial: 25 Acq On : 17 Jan 2002 12:04 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Chlorophenothane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.50 0.51 ug/1 114521 Chrys ene - dl 2 32.80

of 5 Tentative ID MW MolForm CAS# Qual V Chloropheno thane 352 C14H9C15 000050-29-3 87 2op ’-DDT 3 Mitotane 352 C14H9C15 318 C14H10C14 000789-02-6 83 000053-19-0 74 ( 4 l,l-Dichloro-2,2-bis(p-chlorophenyl 318 C14H10C14 000072-54-8 72 Abundance Scan 2881 (31.496 min): 31466.D (-) m/z 234.95 100.00% 235 165 5000

199 36 51 75 99 11 136 31.20 31.40 31.60 31.80

m/z-> ------Am 14.. 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 282 ,fi...1।।11 rn/z 236.95 62.80% Abundance #73698: Chlorophenothane 235

/ 5000 T u- 165 31.20 31.40 31.60 31.80 199 m/z 165.00 55.19% 88 35 281 354 m/z-> ■ ■ i ■ ■ •' i ■ ■ 40 i •1 “ i" ■■i■ “ ■i■■■■i• 11/1111+214 + 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 • i • • ■. fi ■ ■ ■ i ■ • ■ • i■. ■ ■ i • ■. ■ i ‘

Abundance T " ...... " #92obe p. 235

31.20 31.40 31.60 31.80 5000 m/z 199.05 17.94% 165 • 1 100 ........................... 124......... [......... 214 ............... 281...... 319...... 354 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #45306: Mitotane : 235 31.20 31.40 31.60 31.80 m/z 176.05 15.41% 5000 165

88 199 '' I ‘" I' mmmm 14.214.42250 ■ ■ i'1 “ 111" i •' ■11 “ ■ ■ i " ■' 11 • * । । . j * * * * । * * ' > । * * miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.20 31.40 31.60 31.80

31466.D GCMS0103.M Thu Feb 07 12:42:38 2002 Page 3

NYC-WTC_000018414

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NYC-WTC_000018414Source: NYC Law Department, mirrored locally

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