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GCMS analysis results for sample AD27628, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27628 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033159–000033176

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27628 .D Vial: 18 Acq On : 20 Dec 2001 1:24 pm Operator: GALOS Sample : gems unknown. 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Octane, 4-ethyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

35.69 0.69 ng/uL 92433 Perylene-dl2 37.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octane, 4-ethyl- 142 C10H22 015869-86-0 25 2 1-Decene, 2,4-dimethyl- 168 C12H24 055170-80-4 17 3 Isooctane, (e thenyloxy) - 156 C10H20O 037769-62-3 14 4 2-Undecene, 2,5-dimethyl - 182 C13H26 049622-16-4 12 Abundance 5 Scan 3364 (35.689 min): 27628.D (-) m/z 185.10 100.00% 185 57 70 5000 - 43 112 84 98 T‘T 135 207 281 35.40 35.60 35.80 36.00 i 1 ' ' ' i1 ' 1 xJlUj i ■ 1 ' ' i 1 r ■ j - I m/z 57.10 ’ 67.09% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 'Abundance #8095: Octane, 4-ethyl- 57 WA MUW 5000- 71 35.40 35.60 35.80 36.00 85 90 112 m/z 70.05 54.96% 27 42 1 1 11 142 1 1 * 1 1 1 1 1 m/z— > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #14795: 1-Decene. 2,4-dimethyl- 43 57 । L ■ ■ i • ' ■ ■ i ' AMMAA—— 35.40 35.60 35.80 36.00 5000 I 83 m/z 71.05 47.64% s 70 112

. . 1 97 . 168 m/z-> Abundance 20 i 1 ' ' ' i 1 ' 40 1’1111 11’11 1llt1113tn-p-rII11I11 TTETE-T--r111111111111 —T 60 80 100 120 140 160 180 200 220 240 260 280 #67294: Isooctane, (ethenyloxy)- MmAAAbaLel 57 35.40 35.60 35.80 36.00 m/z 43.10 45.15% 71 5000-

27 42 84 MwnW W i ■ ■ ■ > । • i ■ • ■ ' i ' 971..................................... 110

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 35.40 35.60 35.80 36.00

27628.D NP112701.M Fri Dec 21 09:19:24 2001 Page 9

NYC-WTC_000033175

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NYC-WTC_000033175Source: NYC Law Department, mirrored locally

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