GCMS analysis results for sample AD28044, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28044 conducted on January 2, 2002.

NYC-WTC_000034516–000034526

Folder label: “GCMS X 11/21/01 A 12/21/01”

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NYC 9/11 Public Portal Document

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Data File : C: \HPCHEM\ 1 \DATA\DEC2101\28044.D Vial: 35 Acq On : 22 Dec 2001 1:12 am Operator: GALOS Sample : gems unknown 11/21 Inst • : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.62 13.43 ng/uL 3495410 Perylene-dl2 37.17

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 2 4-Undecanol/7-ethyl-2-methyl- 214 C14H30O 000103-20-8 25 3 2-Undecene/ 4,5-dimethyl - , [R@,S@-( 182 C13H26 055170-93-9 25 4 Octane, 111-oxybis- 242 C16H340 _________ 000629-82-3 14 Abundance ........ Scan 3357 (35.622 min): 28044.D (-) !il m/z 185.10 100.00% 185 57

5000 70 43 112 83 gg 125 143 166 203 35.20 35.40 35.60 35.80 36.00 255268i 297 315 T TTTT 1fr t I . ll I ■ i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ r ■ ■ ■ i . .. ....’ r m/z 57.10 75.24% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

57 — 5000 71 112 35'20 35.40 35.60 35.80 36.00 98 m/z 70.15 49.16% i miz- 20 ..... — 100 120 140 160 180 200 220 240 260 280 300 320 40 60 80 ■ ■ i ■ ■ 125 143 166 I 203 298 316 TICTIT"unng—eng"—u—Trhur

Abundance #264 16: 4-Undecancl, 7-thyl-2-methyl- 57 —IPPPPT II -PPP 35.20 35.40 35.60 35.80 36.00 5000 ; 70 m/z 71.15 44.73% 27 r

m/z—> Abundance 5. — 20 40 60 84 112,25 154 196 r p-n-rp-n TI tttt J n-rr.-m-p - , TIT 80 100120 140 160 180 200 220 240 260 280 300 320 #18485: 2-Undecene.’4,5-dimethyl-, [[email protected]@-(Z)]- ।>•>■।■•■■। ■ | ■ ■ • ■ | > ■ > ■ | ■

................ ... ............... 43 57 35.20 35.40 35.60 35.80 36.00

1 rn/z 55.10 40.68% 5000-

84 98 112 140 — ' I1 I 1'1' 111 ■ i ■ • 182 n-pn i . T‘‘‘I0—I0—uTITr , n-p 1 T . T rm-p- m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.20 3540 35.60 35 80 36.00 1

28044.D NP112701.M Thu Dec 27 08:38:11 2001 Page 2

NYC-WTC_000034525

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NYC-WTC_000034525Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD28048, Jan 2002 · Box DEP Box 22

NYC-WTC_000034537

Laboratory report documenting GCMS analysis of sample AD28048 conducted on January 2, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999