GCMS analysis results, sample AD28322, Jan 2002

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GCMS analysis results for sample AD28322 dated January 3, 2002, showing surrogate compound results.

NYC-WTC_000035528–000035539

Folder label: “GCMS X 11/28/01 A 12/28/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 801\28322.D Vial 12 Acq On : 28 Dec 2001 5:57 pm Operator GALOS Sample : gems unknown 11/28 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ***************************** **************************************** Peak Number 3 Decanedioic acid, bis(2-ethylh Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.70 293.56 ng/uL 45182200 Perylene-dl2 37.20

Hit# of .5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 83 2 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 32 3 [1,11-Biphenyl]-4-ol, 3-amino- 185 C12H11NOi 001134-36-7 27 4 4-Undecanol, 7-ethyl-2-methyl-_____ 214 C14H30O _______ 000103-20-8 17 Abundance Scan 3365 (35.696 min): 28322.D (-) m/z 185.20 100.00% 185 57

5000- 112 1 83 pr-r-r-r-j-T-r

m/z-> m LL 3 143 166 203 223242 268 297315 340 369 397 427 — TTITTUTTITTTTTTTTTTTTTTTTTTTTT’’’’ 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380400 420 35.40 35.60 35.80 36.00 m/z 57. 0 67.74% Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000- 57 112 35.40 35.60 35.80 36.00 m/ z 70.15 43.28%

m/z-> 1. 143 166 ." I" •' I • •" 11"' l.. ITO 203 ■ T" " i i■ i 298316 TUUUNUuu—nu—n—gngp 40 60 80 100120140 160180200220240260280300 320340 360 380400420 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 I ■ ' ■ • i ■ ■ 35.40 35.60 35.80 36.00 5000 112 m/z 55.10 39.56% 83 i i 199217 i" ‘ • i • • •' r " • i |11'1 r11' i' *'111"111"' i ‘11 ‘ i1 ’'1111' ‘ i'1" i1'" I'''' i"'11'11111' ’11'1 r' i'''11 miz-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 ... 2.. Abundance

5000 - #19199: 1,1‘-Biphenyl]-4-ol, 3-amino- 185 m/z 7 35.40 35.60 35.80 36.00 37.13%

156

m/z~> p TJUTUpTTn 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 11 ii 111. rq-rrn । rrn । rru । rm j r( n । ————— 35.40 35.60 35.80 36.00

28322.D NP112701.M Mon Dec 31 10:15:19 2001 Page 3

NYC-WTC_000035538

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NYC-WTC_000035538Source: NYC Law Department, mirrored locally

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