GCMS analysis results, sample AD28322, Jan 2002

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GCMS analysis results for sample AD28322 dated January 3, 2002, showing surrogate compound results.

NYC-WTC_000035528–000035539

Folder label: “GCMS X 11/28/01 A 12/28/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC2801\28322.D Vial: 12 Acq On : 28 Dec 2001 5:57 pm Operator: GALOS Sample : gems unknown 11/28 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Naphthalenamine, N-phenyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.58 2.10 ng/uL 454355 Chrysene-dl2 33.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Naphthalenamine, N-phenyl- 219 C16H13N 000135-88-6 60 2 1-Naphthalenamine, N-phenyl - 219 C16H13N 000090-30-2 53 3 1,4 -Methanonaphtha ene, 1,4-dihydro 218 C17H14 055028-73-4 50 4 1-Naphthalenaming, N-phenyl- 219 C16H13N 000090-30-2 49 Abundance lean 2698 (29.579 min): 28322.D (-) m/z 219.15 100.00% 2 9

5000- 109 k T I1 I 39 51 63 77 29.20 29.40 29.60 29.80 30.00 - -Ht +84IL, 127 140 153 165 189 204 । I TTT] TIT TTTTTH# TTT m/z 218.15 55.04% mizz-> 30 40 50 60 70 80 90 100 110 120 130 140 150160 170 180 190 200 210 220 Abundance #27421: 2-Naphthalenamine, N-phenyl- 219

5000 TT 1 11 29.20 29.40 29.60 29.80 30.00 51 m/z 217.05 48.53% 77 115 64 | 89 102 127 191 f’U ’I"" I TTTTTTTTTTTTTTTTTTTTTTTTNTUTT TIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 Abundance #27419: 1-Naphthalenamine, N-phenyl- 219 _________ k ' I ' ' 1 1 1 1 • 1 1 I 1 29.20 29.40 29.60 29.80 30.00 5000 m/z 108.65 37.96% 108 85 95 : । 127136 1. 168 188 204 | j > 11 ■ i ■ 11-'r i"111'' *' r'111"' TT 1111 ‘ '11" " I'1'11 I''" I *" ' I' • " 111" 111" t ‘" I'1 • 'T m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 (Abundance #27287: 1,4-Methanonaphthalene, 1,4-dihydro-9-phenyl- ' I ’ • 1 ' I ' 1 I 2 8 29.20 29.40 29.60 29.80 30.00 m/z 115.05 19.70% 5000- 202 141 109 ... L............ 165 189 i।" I ■" -1 * > 11 p • • < । P “ tj l i l i | l l l I | I ■ l i | i l i . [ I "‘"I........ T 1" l •' r"‘i miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 29.20 29.40 29.60 29.80 30.00

28322.D NP112701.M Mon Dec 31 10:15:15 2001 Page 2

NYC-WTC_000035537

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NYC-WTC_000035537Source: NYC Law Department, mirrored locally

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