GCMS analysis results for sample AD28048, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28048 conducted on January 2, 2002.

NYC-WTC_000034537–000034547

Folder label: “GCMS X 11/21/01 A 12/21/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC21O1\28O48.D Vial: 33 Acq On : 21 Dec 2001 11:23 pm Operator: GALOS Sample : gems unknown 11/21 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ************************* * * * * * * ************************************** Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 1 k R.T. EstConc Area Relative to ISTD R.T.

35.62 8.93 ng/uL 2264560 Perylene-dl2 37.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis (2-ethylhexyl) 426 C26H50O4 000122-62-3 74 2 2-Undecene, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 32 3 [1,1*-Biphenyl]-4-ol, 3-amino- 185 C12H11NO> 001134-36-7 22 4 4-Undecanol, 7-ethyl-2-methyl- 214 C14H30O _______ 000103-20-8 16 Abundance Scan 3357 (35.624 min): 28048.D (-) m/z 185.10 100.00% 185 57

5000 70 43 112 83 98 125 143 166 | miz-? — 40 60 L 80 ‘I’1.1’’" |J...i m_ 203 255268 T‘ ‘III ‘ II"11111111071110 100 120 140 160 180 200 220 240 260 280 300 320 297 315 —I-T"IIIT"TTITT 35.20 35.40 35.60 35.80 36.00 m/z 57.10 74.58% Abundance #55661: Decanedioic acid, bis(2-ethylhexy!) ester 185

5000 57 / — 71 112 35.20 35.40 35.60 35.80 36.00 m/z 70" 49.42% 84 98 125 143 166 | 203 298 316 : . . , . i , . . . , । i ■ • । ■ 11''111 '' ■ ‘'i ■ ■ ■ ■ i1 ■ TTTTT I ' '' ' I p-rr. j . . , rpm-p miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #18485: 2-Undecene, 4,5-dimethyl-, [[email protected]@-(Z,] 43 57 71 35.20 35.40 35.60 35.80 36.00 5000 m/z 71.15 44.69%

84 98 112 140 iI ‘‘9′111■ p-T L 1; I 182 11 •' ' i ■i 1**1′111111’ r’1• n * • । > । • • • • । • • ।»11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #19199: [1,1‘-Biphenyl]-4-ol, 3-amino- / T i ■ ■ ■ ■ i ■ ■ 185 35.20 35.40 35.60 35.80 36.00 m/z 55.10 41.80% 5000

139 156

miz-> — ......... 1134— I1 1 1 I r 1 1 ' I ' ‘ | । । । । । । । 1 1 ’' ' 111''I'> <•।•<••।> < < • । 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.20 35.40 35.60 35.80 36.00 t•q । < > । 11 । । । । ।

28048.D NP112701.M Thu Dec 27 08:39:19 2001 Page 2

NYC-WTC_000034546

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NYC-WTC_000034546Source: NYC Law Department, mirrored locally

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NYC-WTC_000034516

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