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GC/MS analysis results for sample AD23343, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23343 conducted on October 16, 2001.

NYC-WTC_000088535–000088555

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23343.D vial: 16 Acq On : 10 Oct 2001 3:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Undecane, 5-methylene- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

29.51 0.41 ug/1 38344 Chrysene-dl2 33.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane, methylene- 168 C12H24 005698-48-6 27 2 Cyclobut^one, 3,3-dimethyl- 98 C6H10O 001192-33-2 27 3 Cyclob^ane, l-hexyl-2,3-dimethyl- 168 C12H24 055170-84-8 25 4 Cyclopropane, l-butyl-2-(2-methylpr 154 C11H22 041977-35-9 25 Abundance Scan 2666 (29.513 min): 23343.D (-) m/z 56700 100.00%! 53

5000 41 73 129 29.20 29.40 29.60 29.80 ... m/z sYTOO 42745% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 ft Abundance #14771: Undecane, 5-methylene-

5000 . Ai,. .A I A ,V| .......... 29.20 29.40 29.60 29.80 69 m/ Z 41.05 37.00% 27 42 I I I ' ' ' ' I ' 20 40 60 80 100 120 140 160 180 200 220 240 260 iKbundance #1275: Cyclobutanone, 3,3-dimethyl- 53

41 ^■20 29.40 29.60 29.80 5000 m/z 43705 74795% 70

83 98 It 'I' Ti/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #14719: Cyclobutane, 1-hexyl-2,3-dimethyl- A ft AA A 53 29.20 29.40 29.60 29.80 m/z 73.00 33708%

88518!

70 42 , I il 112 126 139 nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 29.20 29.40 29,60 29.80

23343.D NP091101.M Thu Oct 11 13:05:38 2001 Page 6

NYC-WTC_000088547

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NYC-WTC_000088547Source: NYC Law Department, mirrored locally

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