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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087034
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2601\22549.D Vial: 3 Acq On ; 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1-Undecene, 2-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

29.70 1.08 ng/uL 82418 Chrysene-dl2 33.30 Hit# of 5 Tentative ID MW MolForm CAS#

1 1-Undecene, 2-methyl- 168 C12H24 018516-37-5 X 2 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 1 3 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 9 4 Cyclopentanecarboxylic acid, 2-amin 129C6H11N02 037910-65-9 9 Abundance Sea,' . 2711 (29.697 min); 22549.D (-) m/z 56.10 100.00% 53

5000 43 73 ' ' I ' ' ' ' I ' ‘ ' I

I ' ' ' ' I III !?’ «,«? '...................... 239 29,40 29,60 29,80 30,00 m/z 57710 49.29% T)^-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #14760:1-Undecene, 2-methyl- 53

......... L VII,, 1, 11.1 5000 29,40 29,60 29,80 30,00 69 m/z 43.10 36.95% 42 'pill 7'-'-' ‘' H. jy?... ..... nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance ' #28775: Pentadecane, 8-methylene- 55

29,40 29,60 29,80 30,00 5000 69 m/z 41.10 36.09%

27 I .1, Y.IT.TT......... 196,, 224 I' ’'' I'' ' ' I ’ ‘ ' ■ I T I I . I I I 1 1 I I . . ■ ) ■ I , , I , . . . I . I . . , . > ' ' I ' ' ' ' I ' ' ' ' I ' Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Sundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- ......... 5|5 29,40 29,60 29,80 30,00 m/z 55.10 29747%

5000

30 69 82 100 129 ,,,1 ,42 ..... HI... Ti^-> 20 40 60 80 100 120 140 160 180 200 220 240 260 29.40 29,60 29.80 30,00

22549.D NP072501.M Mon Oct 01 14:40:28 2001 Page 5

NYC-WTC_000087034

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