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GC/MS analysis results for sample AD22549, September 2001

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Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\l\DATA\SEP2601\22549.D Vial: 3 Acq On : 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr; 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 6.92 0.68 ng/uL 69471 1,4-Dichlorobenzene-d4 11.99 it# of 5 Tentative ID MW MolForm CAS# Qual ^Hexanol 102 C6H14O 000626-93-7 74 2 ^exanol 102 C6H140 000626-93-7 74 2 -I^xanol 102 C6H14O 000626-93-7 74 2-H^anol 102 C6H140 000626-93-7 64 Abundance Scan 227 (6.918 min): 22549.D (-) m/z 45.10 100.00% 4|5

5000

69 6.60 6.80 7.00 7.20 I 56 I 8487 m/z 43.10 17731% I" " I TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 4)5

5000 _6;6o_a8o_zog_^2o__ 69 m/z 69.10 15.40% 8487 I........ . TlZZ-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583: 2-Hexanol 4|5 II 6.60 6.80 7.00 7.20 5000 "mTz 41.05 13.24%

69 Y 31 39 42 5558 8487 I" " n ........ 111 i-i 11111.... .Ill ......................... I H " I " I I I I " I I . I "I " " I " n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582:2-Hexanol 6.60 6.80 7.00 7.20 "mTz 44.00 12.28% 5000

27 69 19 31 57 I 8487 ... I " " I . .......... .............. . TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.60 6.80 7.00 7.20

22549.D NP072501.M Mon Oct 01 14:40:28 2001 Page 4

NYC-WTC_000087033

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NYC-WTC_000087033Source: NYC Law Department, mirrored locally

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