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GC/MS analysis results for sample AD22552, Sept 2001

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Laboratory report documenting GC/MS analysis of sample AD22552 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087068–000087087

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087079
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2601\22552.D Vial: 6 Acq On : 26 Sep 2001 4:15 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 3 3-Hexanol Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.81 0.45 ng/uL 46448 1,4-Dichlorobenzene-d4 12.00 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hej5i^hol 102 C6H14O 000623-37-0 74 2 3-H^anol 102 C6H14O 000623-37-0 74 3 S^exanol 102 C6H14O 000623-37-0 74 ^/3-Hexanol 102 C6H14O 000623-37-0 64 J^ndance Scan 215 (6.807 min): 22552.D (-) m/z 55410 100.00% 5(9

5000 73 43 .... I\^ J \....... 6.40 6.60 6.80 7.00 7.20 m/z 55710 85.75% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 iMjundance #63531:3-Hexanol 5(9

5000 73 ............ I\, j \l\............... 6.40 6.60 6.80 7.00 7.20 43 m7z 73.05 46.79% +t Wt ‘4 +t I " ' ' I " * ' I '' " I' ' " I p tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 iUjundance #63529; 3-Hexanol 5(9

6.40 6.60 6.80 7.00 7.20 31 m/z 43.05 28.86% 5000 73

44 n/z-> a 102 T-t- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 II

Abundance #1762:3-Hexanol 5(9 6.40 6.60 6.80 7.00 7.20 m/z 41.00 21.85% 31 5000 43 73

102 I-'-............ ' I ' ' ’ ' I r* " I " ' ' I " ' ' I " ' ‘ I ' ' ' ' I I I 11 I' •nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00 7.20

22552.D NP072501.M Mon Oct 01 13:03:18 2001 Page 3

‘NYC-WTC_000087d79 '

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NYC-WTC_000087079Source: NYC Law Department, mirrored locally

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