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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087032
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2601\22549 .D Vial: 3 Acq On : 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.

6.80 0.45 ng/uL 45829 1,4-Dichlorobenzene-d4 11.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

3-Hexanol 102 C6H14O 000623-37-0 83 2 \-Hexanol 102 C6H14O 000623-37-0 64 3 3 exanol 102 C6H14O 000623-37-0 64 4 3-5 xanol 102 C6H14O 000623-37-0 43 Abundance Scan 214 (6.799 min): 22549.D (-) Wz 59.10 100.00% 50

5000 73 .................................................... 43 6.40 6.60 6.80 7.00 7.20 PTTirl.lli- I " " I " " I " 11 I Wz 55.10 86.89% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol 5(9

31 .............. A , ,i 5000 43 73 6.40 6.60 6.80 7.00 7.20 m/z 73.05 42.27% p-m-p I'llll....... ___ ___________ 102 TpT-rrp-rTTyTTTTpTTTpTmrpTTTy^^ Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance ' #63531:3-Hexanol 519

6.40 6.60 6.80 7.00 7.20 Wlilil 73 in/z 43.00 24.10% 43

+u nfe-> Abundance V i""pi 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63529:3-Hexanol 50 ' I " '' I " I"'

6.40 m/z iJ 41.10 6.80 7.00 23.14% 7.20

31 5000 73

44 4; 102 I' ‘' 1' ' ‘' I " ' ' I p" Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 TWTJO

22549.D NP072501.M Mon Oct 01 14:40:27 2001 Page 3

NYC-WTC_000087032

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NYC-WTC_000087032Source: NYC Law Department, mirrored locally

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