GC/MS analysis results for sample AD22549, September 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2601\22549.D vial: 3 Acq On : 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS unknown Inst ; GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.67 1.14 ng/uL 115839 1,4-Dichlorobenzene-d4 11.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 '^exanone 100 C6H12O 000591-78-6 90 2 2 -Ilexanone 100 C6H12O 000591-78-6 90 3 2 -Htexanone 100 C6H12O 000591-78-6 90 4 2-H^anone 100 C6H12O 000591-78-6 83 Sundance Scan 200 (6.671 min): 22549.D (-) m/z 43.00 100.00% 4)3

58 5000

'• 11"' I" " I" ”85I" " I" " I""100 ' I" " I" " I" " I"' 1111111" " I''" I' 11' I ” " I" " 71 I'"' I" " I 6.40 6.60 6.80 7.00 m/z 58.10 56.79% ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance #63384; 2-Hexanone 43

5000 58 6.40 6.60 6.80 7.00 29 m/z 41705 16.48% I '■'-'-'■I 'III...... 71 85 100 11'"I nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance • #63385:2-Hexanone 43

6.40' 6.60 6.80 7.00 5000 58 m/z 57.05 15.88% 29 71 85 100 Ti/z-> V "I'Uh... |l'"i • I ' ’ " I I I' ITT-' r| ■'I'"''...........I.......... . 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone 43 _64p__a60_6j0_7;b0^_ m/z 39700 9.77% 552 58 A

J 29 'I'.. ■■|illi|..,,| 71 85 '' I'' " I' 11" ' I'''' I'''' I'''' I " '' I "'' I'' " I'''' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.40 6.60 6.80 7.00

22549.D NP072501.M Mon Oct 01 14:40:26 2001 Page 2

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