Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
NYC-WTC_000018287–000018315Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\JAN1 802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Hexane, 2,2,5,5-tetramethyl- Concentration Rank 16
R.T. EstConc Area Relative to ISTD R.T.
12.33 0.60 ug/1 227247 1,4-Dichlorobenzene-d4 11.49
Hit# Of 5 Tentati ID MW MolForm CAS# Qual l Hexane, 2,2,5,5-tetramethyl- 142 C10H22 001071-81-4 53 2 Undecane, 2,5-dimethyl- 184 C13H28 017301-22-3 50 3 Decane, ,2,3-trimethyl- 184 C13H28 062338-09-4 47 4 Undecan , 2,6-dimethyl- 184 C13H28 017301-23-4 47 Abundance / Scan 793 (12.326 min): 30986A.D (-) m/z 57.00 100.00% 57
5000
h| 43
■ I | l > I 11 ! I | A pirr 71
150 85 99 113 127 ANA —। । 111111 ■ । r > । > । । > f । r 1I r
m/z 12.00 12.20 12.40 12.60 56.00 48.80%
_A >i|i-ili.|ii.i|iii.|llni|iii-i| 111' ' I' 1 ' ' I ' ' '1 I' ' ' ' n-n-r-p- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #66226: Hexane, 2,2,5,5-tetramethyl- 57
5000 41 71 12.00 1220 12.40 12.60 ' m/z 43.05 36.79% , 85 ‘ i “ “ i1 “ ■ i ■ ‘ “ i ■1127
JWNN ‘ I • • • • | ‘ l11 " i ■ “ ‘i1 ■ • • j ■ ''' I “ “ i •1 “ i111 ‘ ‘ ■ i ■1 “ i1 ■ • ■ i ‘
m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19056: Undecane. 2,5-dimethyl- 57 FTmmmamuBBTmTTTTT 12.00 12.20 12.40 12.60 5000 43 m/z 41.05 33.06% 71
m/z-> Abundance 85 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 57 99 112
#19005: Decane, 2,2,3-trimethyl- 140 184
ANWN m/z 12.00 12.20 12.40 12.60 71.00 27.96%
m/z~> 5000
27 42 +mp71 85 TIWTTnT ' 111'11'' 126 97 1110101820011121190110001B3TBTCTSST818033] 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .AAN 12.00 12.20 1240 12.60
30986A.D GCMS1126.M Tue Jan 22 10:17:48 2002 Page 6
NYC-WTC_000018300
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
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NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
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NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
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NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder