GCMS analysis results for sample AD30486, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30486.D Vial: 21 Acq On 1 Jan 2002 6:23 am Operator: 209 GALOS Sample gems scan 12/14a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.61 3.83 ug/1 1017280 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Ethyl fommamide 73 C3H7NO 000627-45-2 9 2 Silane,tetramethyl- 88 C4H12Si 000075-76-3 9 3 Pent e, 3- methoxy- 102 C6H140 036839-67-5 9 4 1-Bu.tanamine, 3 -methyl - 87 C5H13N _ 000107-85-7 7 Abundance Scan 280 (7.611 min): 30486.D (-) m/z 73.00 1 00.00% 73

5000 43 - 1 i 1 1 381, ] 49 55 61 87 , 87 103 7.20 7.40 7.60 7.80 8.00 m/ z 43.0,5 32.79% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 I ■ ■ ■ ■ i 1 1 1 'i 1 1 ' 1 TFT * 44 58 7.20 7.40 7.60 7.80 8.00 m/z 45.05 11.67% — ‘ I 1 ' ‘ ' 1 1 ' 1 • । । H । i i rr। i i । > i i i ( i i i i । i iri । r-i miz-> 10 20 :30 40 50 a) 70 80 90 100 110 Abundance #845: Silare. tetramethyl- 73 ■p n IT’t. Hi i 1AIm"a i , । i i 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 11.45%

45 15 31 55 88 ‘ ‘ I ‘ ' 1 ‘ I * ‘ * I * * ' • I । ‘ » I ‘ 1 * * | < |>"| ri i । । i r • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i • 1 im/z—> 10 __ 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.72% 5000 45

> » j « i i y 27 33 39 • r * 55■11 > 11 • • । r । ! i i t | IBOBgntn 1 ■ ■ i ‘ 1 • ■ i ■ 1 ■ 1 I 1 1 ' 1 I 1 1 1*4114**11*** ' pF' 1" । miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30486.D GCMS1126.M Tue Jan 15 14:51:12 2002 Page 1

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