GCMS unknowns report for sample AE12281, June 2002

Machine-extracted title · confidence 100%

Report documenting analysis for unknown compounds and surrogate recovery in sample AE12281.

NYC-WTC_000013740–000013750

Folder label: “GCMS X 5/23/02 A 5/30/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2902\12281.D Vial: 22 Acq On : 30 May 2002 7:58 am Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Benzeneethanamine, N-[(pentafl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.68 2.89 ug/1 304830 Naphthalene-d8 15.69 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Benzeneeth amine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 43 2 Cyclopenta! iloxane, decamethyl- 370 C10H30O5Si5 000541-02-6 42 3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 4 N-(Trif/uoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance Scan 1050 (14.682 min): 12281 .D (-) m/ z 73.00 100.00% 73

5000 267 355 -r-r-]-r-r ' 1 I ‘ 1 45 14.40 14.60 14.80 15.00 , 89 108 133 154170, 193208223 251 323339 | f TTI —TTmmnpfunm—mmmpmmmmmmumTPHT Il . TTT m/z 266.95 36.07% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-K(pentafluorophenyl)methylene] 73

5000 267 14*40 14.60 14.80 15.00 44 m/z 355.10 29.37% 1.4... ... 151 179194299.... 250 ....... ...... . miz-> 40 60 80 100 120 146 160 180 '266' 226' '246' 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 14.40 14.60 14.80 15.00 267 m/z 356.10 9.94% 5000

’ 1 i ■ " ■ i ■' ■ ■ i ■' ‘11 ■ ■ ■ ■ i" • • i 191207 i ■ “ ■ i " " i 2511 323339 i■ " ‘i•■ ■ ■ 1’“ ■ ■ i ■ ■ TTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 14.40 14.60 14.80 15.00 m/z 267.95 9.59% 5000 355 44

m/z-> X—488 193 130147 TDuummmaumUmTpT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 267 294 14.40 14.60 14.80 15.00

12281.D GCMS0528.M Thu May 30 10:39:19 2002 Page 2

NYC-WTC_000013748

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000013748Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS unknowns report for sample AE12282, June 2002 · Box DEP Box 15

NYC-WTC_000013751

Report documenting analysis for unknown compounds and surrogate recovery in sample AE12282.

1 shared topics · Same agency, volume and box · similarity 0.999