GC/MS calibration report, Nov 8 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\LB.D Vial: 2 Acq On : 9 Nov 2001 1:14 pm Operator: 2 09 GTkLOS Sample : 10/23 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.84 ug/1 716655 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Te^ltative ID MW MolForm CAS# Qual 1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 MorphoJJme, 4-methyl- 101 C5H11NO 000109-02-4 9 4 3-Hydrt^xy-2-pentanone______________ 102 C5H10O2 003142-66-3 9 Abundance / Scan 288 (7.686 min): LB.D (-) m/z 42/95 10^700% / 40

59 5000

101

nfe-> 10 20 30 40 50 51 4.. 60 70 80 90 7 ' ' ' ' I ' 100 110 _740_^,6g__A80_8t0^_ m/z 5^705 50.24% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 22.65% 15 31 101 I I 1 83 I rT+ r-r-r-r+ ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 40

7.40 7.60 7.80 8.00 SEE 57 m/z 58.05 17.23% 101 15 27 I ' I ■' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ' I ' ' ' ' I ' ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine. 4-methyl- .................... 40 7.40 7.60 7.80 8.00 m/z 41.05 7.45%

5000

■nlz-> 10 15

20 27

30 40 50 56

60 71 101 r Ji ' ' ' I ' ' ' ' I ■ I I I I I ' ' I I '

70 80 90 100 110 7.40 JL^ 7.60 7.80 8.00

LB.D NP103001.M Tue Nov 27 12:31:27 2001 Page 1

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