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GCMS analysis results for sample AD25791, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25791 conducted on November 29, 2001, noting other unknown compounds.

NYC-WTC_000069939–000069949

Folder label: “GCMS Scan X 10/26/01 An 11/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25791.D Vial: 21 Acq On : 17 Nov 2001 10:32 am Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.06 ug/1 367793 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 000123-42-2 50 116 C6H12O2 2 Morpholine, 4-methyl- 000109-02-4 9 101 C5H11NO 3 Acet^e 000067-64-1 9 58 C3H6O 4 Ace^c acid, cyano-, 1,1-dimethylet 141 C7H11NO21 _____ 001116-98-9 9 Abundance Scan 288 (7.687 min): 25791 .D (-) Tm/z 43.00 100.00% 4(3

5000

............ 3? I -y-r-r-i-T—|—r-r-r-r-]—r-r-r-r-p 59

69 101

' ' I I I ' ' I I m7z 7.40 ,L, 7.60 59.05 7.80 8,00 50.87% ■n/z-> 10 20 30 40 50 60 "to ' 'so ' ' 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 '7.40' '7.60 '7.8O 8.60 ' ' 59 m/z 100.95 21.53% 27 101 83 ■ --rl I J' ' ' ' I 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640; Morpholine, 4-methyl- 4(3 , , J - I , , I ,, , I I , , , r I , - I , 7.40 7.60 7.80 8.00 5000 in/z 58.05 17.66% 101 15 71 I T—M 27 ........ ll..................... ......... Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #eZ322: Acetone 4(3 7.40 7.60 7.80 8.00 m/z 41.05 8.49%

5000 58 27 .................... |l''l - '' '5'0' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ ' I ■n^-> 10 20 30 40 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25791.D GCMS1126.M Thu Nov 29 12:20:46 2001 Page 1

NYC-WTC_000069948

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NYC-WTC_000069948Source: NYC Law Department, mirrored locally

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