Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
NYC-WTC_000086788–000086807Folder label: “508 Scan 9/15/01 9/26/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0101\LBC .D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************************************************************ Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 11.64 0.54 ug/1 80259 1,4-Dichlorobenzene-d4 11.79 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1,4-Di^lorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzenfe-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 35 3 Benz^dehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 2-MeXhyl-6-nitroaniline 152 C7H8N2O2 ______ 000570-24-1 10 Sundance Scan 719 (11.640 min): LBC.D (-) m/z 149.90 100.00% 1!l0
5000 115
52 78 11.40 11,60 11,80 12.00 38 ' ' I I I 11 I ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 11111111111'' 4^ m/z 151.90 66.15% ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0
5000 115 78 11.40 11.60 11.80 12.00 52 rn/msTOO 34.8 8"% -n/z-> 30 35 ' I ' ' ' ' I ' ' ' ' I ' 40 50 60 .,..11,..? 70 80 ......... 1,1.......... 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0
115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 18.93%
35 I I I ' ' ' I I ' ■Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- I 1!12 11.40 11.60 11.80 12.00 m/z 52.00 14.91% 106 5000 53 81
122 ' I ' ' '' I ' ' ' ‘ I ' ' '' r 92 ' I I ' ' ' I ' 136 I, ■nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 1 2.00
LBC.D NP091101.M Tue Oct 02 12:17:19 2001 Page 5
NYC-WTC_000086798
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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