Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
NYC-WTC_000086788–000086807Folder label: “508 Scan 9/15/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT0101\LBC.D vial: 3 Acq On : 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample : 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 6 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.54. 0.89 ug/1 158195 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Butyl h^adecanoate 312 C20H40O2: 000000-00-0 42 2 Piperic^n-4-carboxylic acid 129 C6H11NO2: ' 000498-94-2 35 3 Cyclobutane, 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 4 1-Hex/ne, 2-methyl-_____________ 98 C7H14 006094-02-6 27 Abundance / Scan 2669 (29.541 min): LBC.D (-) Tim/z 56.00 100.00% 55
552 4' 73 257 129 239 29.20 29.40 29.60 29.80 312 I' ' ' ' 1' TrTp-myTVTVYrTVfjT'TbnjTTTT'jTTTnyTHn-ryTTTH-pTTn^ m/z 57.00 55.30% 'n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55
5000 258 29.20 29.40 29.60 29.80 240 312 m/z 43765 37.39% 129
■n/z-> I' ''' I ‘ 20 40 It 60 I' ’ I'' ’' I • 11 r 11 ■ 1 1111 1111 11.) ■ ■ ■
80 100 120 140 160 180 200 220 240 260 280 300 214 P’’' ‘ I p-r-n-p-r-rry
/Abundance #5228: Piperidin-4-carboxylic acid 55 ' ' i ' ' ' ’ I ' 29,20 29.40 29,60 29.80 5000 m/z 41.00 35.22% 30 84 129
Tl/Z-> r 20 40 60 X I' ‘' r ''' r ''' r ''' r ‘' I'' ’' r ''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 55 _292g_j9;40_^,60_ja8g___ in/z 73700 32.02%
5000
27 70
■n/z~> I U m I' '' ' I' 9/ 111125140 . ............ 168 196 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 pm-rp T / \ I ' ' ' 'I 29.20 29.40 29.60 29.80
LBC.D NP091101.M Tue Oct 02 12:17:24 2001 Page 6
NYC-WTC_000086799'
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NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for TCLP analysis including retention times and response factors for various compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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Series of administrative records documenting Section 508 accessibility scans conducted at the World Trade Center site between September 15 and 26, 2001.
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Standard operating procedure for liquid-liquid extraction specifying drip rates and reagent lot numbers.
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Laboratory results for sample AD22491 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22492 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.
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