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GC/MS calibration table, Oct 2001

Machine-extracted title · confidence 50%

Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.

NYC-WTC_000086624–000086643

Folder label: “508 Scan

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Scanned page image, NYC-WTC_000086635
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0101\LBC.D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOS Sample 9/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.54 0.89 ug/1 158195 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl h^adecanoate 312 C20H40O2: 000000-00-0 42 2 Piperic^n-4-carboxylic acid 129 C6H11NO2: 000498-94-2 35 3 CyclobiAtane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 4 1-Hex^e, 2-methyl- 98 C7H14 006094-02-6 27 Abundance Scan 2669 (29.541 min): LBC.D (-) m/z 56.00 100.00% 55

5000 4' 73 257 I 101 ^29 239 29.20 29.40 29.60 29.80

n^-> i-rmY- 20 40 .. 60I.J,.80 100 120.1. 140 160 180 200 220 240I 260, 280 300312 m/z 57.00 (' ’ ’ ’ I'' ’ ‘ I ‘ I 55.30% Abundance #44549; Butyl hexadecanoate 53

258 , . I . , . . I , di 11 . I 5000 29.20 29.40 29.60 29.80 240 312 m/z 43.05 37739% 129

tt7z-> 20 40 Ji 60 IrI 11... 11.1r J I I I 11 157171^^ I''''I 214 80 100 120 140 160 180 200 220 240 260 280 300 ^kbundance #5228; Piperidin-4-cartx3xylic acid 53

29.20 29.40 29.60 29,80 5000 m/z 41.00 35.22% 30 84 il ^29 II 100 i ' I'''' I'''' I ’''' I'''' I'''' I'''' r ''' I'''' I'''' I I''''' i" ''' I'''' I' ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 53 29.20 29.40 29.60 29,80 m/z 73.00 32.02%

5000

27 70 I I, I, 9/ 1111251^ 168 196 I' ’'' I ‘ I., I r., I). ,1,11.1.1..., I. I n 1.1.11 I I I I . I I I I I I . » n I T T T)ZZ-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

LBC.D NP091101.M Tue Oct 02 12:17:24 2001 Page 6

NYC-WTC_000086635

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NYC-WTC_000086635Source: NYC Law Department, mirrored locally

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