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GC/MS calibration table, Oct 2001

Machine-extracted title · confidence 50%

Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.

NYC-WTC_000086624–000086643

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086636
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0101\LBC .D Vial: 3 Acq On 1 Oct 2001 3:40 pm Operator: 209 GALOf Sample 9/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecanoic acid, butyl ester Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.67 0.67 ug/1 119499 Chrysene-dl2 33.16 Hit# of Tentative ID 5 MW MolForm CAS# Qual <2^ Octadecanoic acid, butyl ester 340 C22H44O2i 000123-95-5 80 2" Butyl tetradecanoate (myristate) 284 C18H36O2i 000000-00-0 72 3 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2i 000646-13-9 64 4 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 35 Abundance Scan 2901 (31,671 min): LBC,D (-) Tm/z 56.00 100.00% 53

5000 4 73 129 285 31,40 31,60 31,80 32,00 m/z 57.00 50.23% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Sundance #73570: Octadecanoic acid, butyl ester

5000 7^^ 285 340 31,40 31,60 31,80 32,00 73 129 267 in/z 43.05 42.38% 185 241 aS”,1.1... I I' ■' H''' Ti^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

31,40 31,60 31,80 32.00 5000 m/z 41.00 33.83% 229 129 211

•nZz-> '' I'' 40 1,1 y IffJ?..................... ■pTT*TyrrTTYT-rTfyTrTTyTrTTTrYrTTTp^ 60 . T. . 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid. 2-methylpropyl ester 57 31,40 31,60 31,80 32,00 m/z 73.00 31.39% 5000 285 267 J 1^5 241 [ I 340 I'''' I'''' I''' ‘ i''''' I'''' I ' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31,40 31,60 31,80 32,00

LBC.D NP091101.M Tue Oct 02 12:17:28 2001 Page 7

NYC-WTC_000086636

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NYC-WTC_000086636Source: NYC Law Department, mirrored locally

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