NYC 9/11 Public Portal Document
Libra:?/ Search Compound Report
Data File ; C;\HPCHEM\1\DATA\OCT0101\LBA.D Vial; 2
Acq On : 1 Oct 2001 2:41 pm Operator: 209 GALOS
Sample : 9/14 Inst : GC/MS 209
Mise Multiplr; 1.00
MS Integration Params; LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library ; C;\DATABASE\NBS75K.L
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Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
7.76 0.56 ug/1 110322 1,4-Dichlorobenzene-d4 11.79
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pent none, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56
2 5-Hex» -2-one 98 C6H10O 000109-49-9 9
3 But e, 1-ethoxy- 102 C6H14O 000628-81-9 9
4 3-a droxy-2-pentanone___________ 102 C5H10O2 003142-66-3 9
^bundan(^e Scan 296 (7.755 min): LBA.D (-) m/z 42.95 100.00%
4b
59
5000-
101
740 7.60 7.80 8.00
.................................... 38 11 Wz 59.05 54.60%
I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I
x\lz-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #3245: 2-Pentanone. 4-hydroxy-4-methyl-
4fe
5000 59
7.40 7.60 7.80 8.00
m/z 100.95 21.53%
31 ftq 101
I I 73 “3 ,1
10 20 30 40 50 60 70 80 90 100 110
Abundance #63205:5-Hexen-2-one
4)3
......................
7.40 7.60 7.80 8.00
5000-
m/z” 58.05 17.12%
L
55
15 27
I I 38 I 50 83 98
' ' I ' ' ' ‘ I ' ' ' ' I ' ' ' ' ' ' I ' ' ' ' I ' ' I U ' ' ' ' I ' I ' ■ ' I I I t . I 1
Tn/z-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #63550: Butane, 1-ethoxy-
5(9 7.40 7.60 7.80 8.00
31 m/z 41.00 8.44%
5000
45 73
I 87 102
I ' ' ' ' I ' ' ' ' I ' I ' I ' ' ' ' I ' ' ' ' I ' ' '' I ' ' ' ' I I ' ' ' I
■n/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
LBA.D NP091101.M Tue Oct 02 12:02:35 2001 Page 1
NYC-WTC_000086774
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