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GC/MS calibration table for TCLP analysis, Oct 2001

Machine-extracted title · confidence 95%

Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.

NYC-WTC_000086768–000086785

Folder label: “508 Scan”

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Scanned page image, NYC-WTC_000086774
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Libra:?/ Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT0101\LBA.D Vial; 2 Acq On : 1 Oct 2001 2:41 pm Operator: 209 GALOS Sample : 9/14 Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L *************************************************************************** Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 7.76 0.56 ug/1 110322 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent none, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 5-Hex» -2-one 98 C6H10O 000109-49-9 9 3 But e, 1-ethoxy- 102 C6H14O 000628-81-9 9 4 3-a droxy-2-pentanone___________ 102 C5H10O2 003142-66-3 9 ^bundan(^e Scan 296 (7.755 min): LBA.D (-) m/z 42.95 100.00% 4b

59 5000-

101 740 7.60 7.80 8.00 .................................... 38 11 Wz 59.05 54.60% I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I x\lz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone. 4-hydroxy-4-methyl- 4fe

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 21.53% 31 ftq 101 I I 73 “3 ,1 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205:5-Hexen-2-one 4)3 ...................... 7.40 7.60 7.80 8.00 5000- m/z” 58.05 17.12%

L 55 15 27 I I 38 I 50 83 98 ' ' I ' ' ' ‘ I ' ' ' ' I ' ' ' ' ' ' I ' ' ' ' I ' ' I U ' ' ' ' I ' I ' ■ ' I I I t . I 1 Tn/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63550: Butane, 1-ethoxy- 5(9 7.40 7.60 7.80 8.00 31 m/z 41.00 8.44%

5000

45 73 I 87 102 I ' ' ' ' I ' ' ' ' I ' I ' I ' ' ' ' I ' ' ' ' I ' ' '' I ' ' ' ' I I ' ' ' I ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

LBA.D NP091101.M Tue Oct 02 12:02:35 2001 Page 1

NYC-WTC_000086774

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NYC-WTC_000086774Source: NYC Law Department, mirrored locally

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