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GCMS analysis results for sample AD24949, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24949 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069117–000069127

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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Scanned page image, NYC-WTC_000069125
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NYC 9/11 Public Portal Document

Librairy Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24949.D Vial: 17 Acq On : 7 Nov 2001 4:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.62 ug/1 317233 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, Lydroxy- 4 -methyl - 116 C6H12O2 000123-42-2 53 2 Acetic acid, ,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 Acetone 58 C3H6O 000067-64-1 12 4 5-Hexen-2 ne 98 C6H10O 000109-49-9 9 Abundance ✓ Scan 289 (7.698 min); 24949.D (-) m/z 42.95 100.00% 4(3

5000 59

101 83 7.40 7.60 7.80 8.00 T' • • • 1 ■ • ' ■ I ' I ■ ITT m/z 59.05 47.35% nfe-> 10 20 30 40 50 60 70 80 90 100 110 AbutKterwe #64275:2-Pentanone. 4-hydroxy-4-methyl- 4(3

5000 59 Zro ZM m/z 101.05^21.71% 15 31 101 I I I 83 1 ' ' ' ' I ' ' ' ' I ''' ' ' I ' [nZz-> 10 20 30 40 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 4^

7.40 7.60 7.80 8.00 5000 57 m/z 58.05 19.32% 101 15 27I Ti&-> Abundance 10 I

20 30 ‘ 11 ' ‘ ‘ I 40

4(3 50 60 ' I ‘ ‘ ‘ ‘ I ' ' ‘ ' 1 ‘ ‘

#62322: Acetone 70 80 ‘ I ‘ 90 ' I ‘ 100 ‘ I 110

7.40 7.60 I ~• I I I ' ' . i-r'i I 1 I rm 1 7.80 8.00 iT-

mTz irToF 7.70% 5000 58 27 ' I ' ' ‘ I ' ' ' ' I ' ' ' ' 1 ' ' ' ‘ 1 ' ■ ' ’ I ' ' ' ' I 10 20 30 40 50 60 70 80 90 100 110 ' 7.^' ZOT 7.ro' 8^

24949.D NP103001.M Fri Nov 16 15:23:41 2001 Page 1

NYC-WTC_000069125

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NYC-WTC_000069125Source: NYC Law Department, mirrored locally

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