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GC/MS analysis results for sample AD23501, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088864
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1601\23501.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 2 09 GTkLOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.46 ug/1 45823 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 :ntative ID MW MolForm CAS# Qual

1 1,4-Dich]/5robenzene-d4 150 C6C12D4 003855-82-1.72 2 Benzo[b/thiophene-4-ol 150 C8H6OS 003610-02-4 32 3 Benze:^-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1-25 4 2-A<^mantanone 150 C1OH140 000700-58-3 23 Abundance/ Scan 717 (11.620 min): 23501 .D (-) m/z 149.90 100.00% 1‘i0

553 115

52 78 38 11.20 11.40 11.60 11.80 12.00 J.,. .,.,■11,...??.. — m/z 151.90 58.10% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 T ' ' I ' ' 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 35.43%

Ti/z-> 30 35 40 50 ' I ' 60 .,..11,..??.. 70 80 90 100 110 120 130 140 150 160 Abundance #9645: Benzo[b]thiophene-4-ol 1!i0

121 11.20 11.40 11.60 11.80 12.00- 5000 “mTz 78.00 18.83%

78 96 ........... l,l|,, 71/Z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0— 11.20 11.40 11.60~ 11.80 12.00 ■m7z“'11679r 15.49% 115 5000 52 78

Tife-> 30 35 I 40 50 ' I ' ' ' ' I ' 60 70 80 87 I 90 100 ... 130 140 „J,I120 110 150 160 .... J\.. 11.20 11.40 11.60 11.80 12.00

23501.D NP091101.M Thu Oct 18 10:21:30 2001 Page 5 .

NYC-WTC_000088864

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NYC-WTC_000088864Source: NYC Law Department, mirrored locally

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