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GC/MS analysis results for sample AD23607, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23607 conducted on October 19, 2001.

NYC-WTC_000088986–000088999

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088998
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23607.D Vial: 14 Acq On : 17 Oct 2001 2:57 am Operator: 2 09 G7VLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.62 0.53 ug/1 54411 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID MW MolForm .. CAS# Qual

1 1,4-Dichlox6benzene-d4 150 C6C12D4 003855-82-1 53 2 Benzo[b]feniophene-4-ol 150 C8H6OS 003610-02-4 23 3 Benzer^l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 4 Benz§Zdehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance < Scan 717 (11.623 min): 23607.D (-) m/z 149.90 100.00% 1!i0

5000- 115 52 78 I ' ' ' ' I ' ‘ ' ' I ' ' 11.20 11.40 11.60 11.80 12.00 .... I' . I■ , . ................................. ,1 m/z 151.90 58.39% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1i«

5000 115 ' ' I ' ' 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 33.52% l„„35... 1 Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance' #9645:’Benzo[b]thiophene-4-ol 1!i0

121 11.20 11.40 11.60 11.80 12.00 5000- "m/z 78.05 18743%

7896 ........ ............. i.L 89 ........ Tl/Z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance — #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- - 1!10 11.20 - 11:40 -11.60 -11 ;80 12.00 “mTz 51.90 . 15.73% 115 -- 5000 52 78

35 87 I I ■■ ' r ' '' I ' ' ' ' I ' I' Tlfe~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160' 11.20 11.40 11.60 11.80 12.00

23607.D NP091101.M Thu Oct 18 10:37:30 2001 Page 5

NYC-WTC_000088998

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NYC-WTC_000088998Source: NYC Law Department, mirrored locally

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