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GCMS analysis results for sample AD28471, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD28471 conducted on December 6, 2001.

NYC-WTC_000034347–000034365

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28471.D vial: 7 Acq On 4 Dec 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclobutane, 1,1-dimethyl-2-oc Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.44 7.24 ug/1 1902670 Chrysene-dl2 33.04 Hitt? of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclobutane/ 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 2 1-Hexene, /-methyl- 98 C7H14 006094-02-6 27 3 1-Hexene/2,5-dimethyl- 112 C8H16 006975-92-4 27 4 1-Heptene, 2-methyl- 112 C8H16 015870-10-7 27 Abundance” ' Scan 2657 (29,438 min): 28471.D(-) m/z 56.00 100.00% 55

5000 41 73 257 101 129 239 —I. . . . 1 . . ■ I f ITTT TT I I I I I

mz-> ________ I "T‘‘T 11 TTr 20 40 lZ 4 115 111157171165199213 283 312 m/z 57.00 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 48.95% Abundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- 55

5000 ' .. LW. 29.20 29.40 29.60 29.80 m/z 41.05 41.35% 27 70 I TT"TTrr —9 111125.................................. ‘I‘ mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 55

29.20 29.40 29.60 29.80 41 m/z 43.00 40.36% 5000 । 27 70 98 1 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ...... . Abundance #64038:1-Hexene, 2,5-dimethyl- 56 29.20 29.40 29.60 29.80 m/z 55.00 31.18% 41 5000 •

m/z—> i LL 70 111'''' I ‘1 20 40 i'1'' l ’ ■' ■ i ■ 60 112 ’ 80 100 120 140 160 180 200 220 240 260 280 300 -A 29.20 29.40 29.60 29.80

28471 .D GCMS1126.M Wed Dec 05 11:27:29 2001 Page 1

NYC-WTC_000034354

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NYC-WTC_000034354Source: NYC Law Department, mirrored locally

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