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GC/MS analysis results for sample AD22653, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Rep<

Data File ; C:\HPCHEM\l\DATA\SEP2801\22653 Vial: 12 Acq On : 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP0911C-1 ' R n-’ T ntegrator) Title : 209 625/TCLP calibration tab'-, ./ ■ 1 Library : C:\DATABASE\NBS75K.L ******************************************* • - * * ■ -.*★*************

Peak Number 13 Heneicosane c'cncentration Rank 10 R.T. EstConc Area Relati'^ o IS j R.T. 36.39 0.59 ug/1 80479 Perylene- 37.28 Hit# Of 5 Tentative ID MW Mo ' orm CAS# Qual (Heneicosane 296 C21 000629-94-7 90 2 Octadecane 254 C.l. 000593-45-3 86 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C2 054833-48-6 86 4 Hexatriacontane_____________________ 507 C3 000630-06-8 86 iKbundance Scan 3415 (36,394 min): 22653,0 (-) 57.00 100.00% 57 i'i 71 43 85 5000

I b I 113 I- '0 36,20 36.40 36,60 36,80 ,, III, ,1, I i,■J, .,4, '*F y.............. : 71.05 74.48% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #42201: Heneicosane 5/ 71 85 5000 ? 35'20 36.-10 36,60 36.80 99 43 .'0 5 63.52% ■•27 141 155 I, n I,, P,, M 266 - 40 60 80 100. 120 140 160 180 200 220 240 260 ; . -0 Abundance #71560: Octadecane 43 57 SA-----

71 6 36,20 36,40 36,60 36,80 5000 85 85.05 53.85%

99 .1.... Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 .00 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- , . (. Y0|YT. I I I I 57 0 36,20 3 .0 36,60 36,80 71 i: z 55 . C ,) 21.07%

5000 I\ 85

.1 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 2 .0 36,20 36 <0 36,60 36,80

22653.D NP091101.M Fri Oct 05 08:57:08 Page 13

NYC-WTC_000087322

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NYC-WTC_000087322Source: NYC Law Department, mirrored locally

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