GCMS results log, sample AD26833, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26833.D Vial: 33 Acq On 7 Dec 2001 4:14 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 13 Hexatriacontane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

36.41 0.91 ng/uL 263538 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 90 2 Pentatriacontane 493 C35H72 000630-07-9 87 3 Hexatriacontane 507 C36H74 000630-06-8 87 4 Tetratetracontane 619 C44H90 _______ 007098-22-8 87 Abundance Scan 3442 (36.407 min): 26833.D (-) m/z 57.10 100.00% I 57

I 5000 85

1 m/z-> ' r 1 50 l 100 150 207, , , , 21 200 250 300 350 400 450 500 36.00 36.20 36.40 36.60 36.80 m/z 43.10 71.47% Abundance #74635: Hexatriacontane 57

_X 5000- 85 36.00 36.20 36.40 36.60 36.80 m/z 71.05 66.79% ■ ■ i ■ 1113.141, . 196 225 253 281.............. m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #58743: Pentatriacontane 57 -AA4PA+4,1........... 36.00 36.20 36.40 36.60 36.80 5000 85 m/z 85.05 43.52%

; | • 113 141 169 197 225 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #59136: Hexatriacontane A A................1........... A A 57 36.00 36.20 36.40 36.60 36.80 |

J m/ z 55.10 29.09% 5000 85

, | Lull111...... ^39..... ..... 379 407 435 , 478 506 DADA AL —A/ miz-> 50 100 150 200 250 300 350 400 450 500 36.00 36.20 36.40 36.60 36.80

26833.D NP112701.M Tue Dec 11 14:46:55 2001 Page 13

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