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GCMS results log, sample AD27009, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27009 completed on December 11, 2001.

NYC-WTC_000032534–000032552

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

•Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Hexatriacontane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

35.55 1.24 ng/uL 480707 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual @ 1 Hexatriacontane 507 C36H74 000630-06-8 2 Dotriacontane 451 C32H66 000544-85-4 3 Dotriacontane 451 C32H66 000544-85-4 86 4 Hexatriacontane_______________ 507 C36H74 000630-06-8 78 Abundance Scan 3349 (35.551 min): 27009.D (-) m/z 57.05 100.00%

T 57

5000 85

35.20 35.40 35.60 35.80 , .11 1. L 113 4141 m/z 43. 0 65.57% m/z-> 50 100 150 200 250 300 350 400 450 'Abundance #74636: Hexatriacontane 57

5000 85 T TT 35.20 35.40 35.60 35.80 m/z 71.05 58.13% i m/z-> -i r—T 50 1123 100 150 141 169 197 200 250 300 350 400 450 Abundance #74490; Dotriacontane i 43 AIA TII TI ■ 71 35.20 35.40 35.60 35.80 5000 m/z 85.15 39.19%

97 127 155 183 379 407 , 450 I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74492: Dotriacontane

. J_ 57 35.20 35.40 35.60 35.80 m/z 55.10 26.58% 5000 85

T 4113 295 323 351 379 450 TII 1 MAA,AA-ANAWAAAMa m/z-> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80

27009.D NP112701.M Tue Dec 11 14:59:44 2001 Page 11

NYC-WTC_000032551

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NYC-WTC_000032551Source: NYC Law Department, mirrored locally

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