GCMS analysis results for sample AD27392, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27392.D Vial: 15 Acq On : 13 Dec 2001 11:06 pm Operator: GALOS Sample : gems unknown 11/14 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Hexadecanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.80 1.11 ng/uL 292879 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexadecanol 242 C16H340 036653-82-4 46 2 Nonadecanol 2 84 C19H40O 052783-43-4 43 3 1-Hexacosanol 3 82 C26H540 000506-52-5 43 4 1-Octadecanol 2 70 C18H380 000112-92-5 38 Abundance Scan 2722 (29.800 min): 27392.D (-) m/ z 43.10 100.00% 43

5000 51 , 83 111 I ' ' ' ' I ' f 1

m/z- 20 i" " “ 40 60 L — TT’TT’TTTT I ’1111 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 i " " i'' " i 29.40 29.60 29.80 30.00 30.20 m/z 55.10 49.09% Abundance #71247: 1-Hexadecanol i 43

5000 83 —........ . ■ ■ i ■ ■ 29.40 29.60 29.80 30.00 30.20 27 m/z 57.10 47.34% 11 T‘111 I t1‘,—01111TTC‘ITTT 196 ‘ 224 I > t | I ! . . | ! I I I | I'*'' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #40237: Nonadecanol 43 A A , ?.................. 29.40 29.60 29.80 30.00 30.20 5000 83 m/z 61.10 44.02% 27 111 266 pi rq m । । । । । t । । । « । । i ■' ■ ■ i I'' ’' I I''1' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #52385: 1-Hexacosanol 43 29.40 29.60 29.80 30.00 30750 m/z 69.10 42.90% 5000 83

61 | 111 -.............................. ...................... ,,, 336,,,364

miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 29.40 29.60 29.80 30.00 30.20

27392.D NP112701.M Fri Dec 14 12:39:26 2001 Page 2

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