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GC/MS analysis results for sample AD22558, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22558 conducted on October 1, 2001, identifying unknown compounds.

NYC-WTC_000087097–000087119

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087115
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2701\22558.D Vial: 2 Acq On : 27 Sep 2001 1:02 pm Operator: GALOS ' Sample : gc/ms unknown <1 ml Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params-. LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetracosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 32.89 1.14 ng/uL 152864 Chrysene-dl2 ' 33.29 Hit# of 5 Tentative ID MW MolForm CAS# Qual

^^Tetracosane 338 C24H50 000646-31-1 90 2 Nonadecane 268 C19H40 000629-92-5 86 3 Nonadecane 268 C19H40 000629-92-5 86 4 Pentadecane 212 C15H32 000629-62-9 86 Abundance 57 Scan 3059 (32.886 min): 22558.D (-) m/z SYTTO ToPToo? 43 71 5000 85

T-p—r 99 32.60 32,80 33.00 33.20 ■p J P ' ' ' P ' ' ' P ' ' ' P ' ' ' P ' '' P ‘ ' P ' ' ' P ' ' ' P ' ‘ ' I m/z43.10 72.62% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 32.60 32.80 33.00 33.20 m/z 71.05 64.69%

n/z-> Abundance 40 "U u. 60 I 99 il "' '' I '' ' ' I '' '' I '' 155169183197 I' f I' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #37469: Nonadecane I' 294 I' ' '' I' ''' I' '' ' I' ''' I 338 I' '' 'I'

57 \\.......... ............ 43 71 32.60 32.80 33.00 33.20 85 5000 m/z 85.05 43.35%

183197 268 p-rT-r-p-TT-r-p I ' '' ' p ' ' ' p ' ' ' I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71948: Nonadecane yr- ..... / 43 57 32.60 32.80 33.00 33.20 m/z 41.10 29.02% 71 gsa 85

268 / 1__ I 156 196210225 ' I ' ' ' ' I ' ‘I " ' 11 " • I ' ' ’' I ' ' '‘ I ' ' •’ I• ' ' ' I I' ' ' ' I ' ' ' ' I' ' ' ' I ' ' ' ' I I ' ' ' ' I n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.60 32.80 33.00 33.20

22558.D NP072501.M Mon Oct 01 14:52:37 2001 Page 11

NYC-WTC_000087115

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NYC-WTC_000087115Source: NYC Law Department, mirrored locally

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