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GC/MS analysis results for sample AD22979, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22979 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087773–000087793

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087788
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\22979 .D Vial: 5 Acq On 3 Oct 2001 4:33 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 9 Heptadecane, 9-octyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

34.63 0.90 ug/1 139973 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 9L 2 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91^ 3 Tricosane 324 C23H48 000638-67-5 91 / 4 Tetratetracontane 619 C44H90 007098-22-8 91/ Abundance Scan 3223 (34.632 min): 22979.0 (-) m/z 57.00 100.00% 57 71

5000

m/z-> ^undance 40 Xu 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #49558: Heptadecane, 9-octyi- '' I' ‘ ‘ ‘ I m/z 34.40 34.60 34.80 35.00 71.10 73.75%

i 57

71 5000 fV 34.40 34.60 34.80 35.00 m/ z 43.0,5 65.34% I I 239 ' ' ' I ' ' ' ' I ' '' ' ' I ' ' 310 •p-TTTy 352 I ‘' I'''' I ‘ ‘' I'''' I I '' ' ' I T,/Z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #51002: Heneicosane, 11-(1-etbylpropyl)- 43 ......... 71 34.40 34.60 34.80 35.00 5000 m/z 85.05 52.04%

183197 225 338 I I I • I ' I I I I r. I 1 I 1 ■ ' I •' • • I'' " I' I I ' ‘ ‘ ' I p-rrrp-rrrj- nn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73318: Tricosane 43 34.40 34.60 34.80 35.00 22.01% 71 5000

183197 225 296 324 I ' '“ ' I T ' ' ' ) > I « I I ' ‘ ' 1 I ' < •'' 1 " •' I ‘' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.40 34.60 34.80 35.00

22979.D NP091101.M Tue Oct 09 09:54:45 2001 Page 9

NYC-WTC_000087788

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NYC-WTC_000087788Source: NYC Law Department, mirrored locally

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