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GC/MS analysis results for sample AD23261, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23261 conducted on October 12, 2001.

NYC-WTC_000088098–000088114

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088112
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23261 .D Vial; 7 Acq On 9 Oct 2001 7:13 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if**************

Peak Number 8 Hexatriacontane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 35.50 0.53 ug/1 77026 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetracosane 338 C24H50 000646-31-1 91 3 Pentatriacontane 493 C35H72 000630-07-9 91 4.Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 3318 (35.505 min): 23261.D (-) m/z 5^700 100.00% 7

71 43 85 5000

35.20 35.40 35.60 35.80 154 208 281 I'' ‘' I'' pn-Tp-r-m-p m/z 71710 67.45% ( Tl/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

71 5000 85 35.20 35.40 35.60 35.80 m/z 43.00 59.10%

■n/z-> 40 60 J 99 y 1,1 \P^?7141 155169183197211 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ft <\bundance #73543: Tetracosane 43 57 71 35.20 35.40 35.60 35.80 5000 85 m/z 85.05 51.35%

99

' ‘ I'' I, , ,i ............................... Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #58743: Pentatriacontane 43 5(7 35.20 35.40 35.60 35.80 m/z 41.05 20.87% 71 5000 85

n/z--> 40 wu I

60 I I 99 55169183197211225239 I'' '' I'' ' ‘ 1 80 100 120 140 160 180 200 220 240 260 280 300 320 340 p-m-p-n-ry 35.20 35.40 35.60 35.80

23261.D NP091101.M Thu Oct 11 10:46:01 2001 Page 8

‘NYC-WTC_bod688Tl 2

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NYC-WTC_000088112Source: NYC Law Department, mirrored locally

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