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GC/MS analysis results for sample AD22652, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087274–000087302

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\l\DATA\SEP2801\22652.D Vial: 11 Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Heptadecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 33.72 1.81 ug/1 276569 Chrysene-dl2 33.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 91\ 2 Heneicosane 296 C21H44 000629-94-7 91 \ 3 Eicosane 282 C20H42 000112-95-8 91/ 4 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 9^ Abundance Scan 3124 (33.718 min): 22652.D (-) m/z 57700 100700% 57

43 71

5000 85

,,ll, .T, T/F 197 211 227239 281 JXt ^.40 33.60 33.80 34.00 , JI i l l I 'I I I I T ( j I I I 111 I |-1 I I I' I I I 'l , , f I I I 'i I I r'l I , I I I I i I I I I I I I I m/z 71710 68764% mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 <\bundance #32063: Heptadecane 5)7

71 85 5000 33.40 33.60 33.80 34.00 99 m/z 43705 65.38% 196 240 n/z-> 40 rJU 60 T -v- 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 J I ' ' 85 33,40 33.60 33.80 34.00 5000 m/z 85.05 46.39% ft 99

■nfe-> 40 uu 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72326: Eicosane JL T' ' ‘ T 57 ^.40 33.60 33.80 34.00 43 m/z 55.00 217^7% 71 5000 85

99 HQ I ,,l y 127141 155169 282 Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 33.40 33.60 33.80 34.00

22652.D NP091101.M Wed Oct 03 11:53:26 2001 Page 12

NYC-WTC_000087292

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NYC-WTC_000087292Source: NYC Law Department, mirrored locally

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