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GCMS analysis results for sample AD26679, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26679 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032028–000032057

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26679.D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************************************************

Peak Number 13 1-Hexene, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

29.57 1.30 ng/uL 275824 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 2 methyl- 98 C7H14 006094-02-6 35 2 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H160 054644-32-5 28 3 2-Methyl-1- tetradecene 210 C15H30 000000-00-0 25 4 1-Hexene, 5-methyl- 98 C7H14 003524-73-0 25 Abundance Scan 2697 (29.572 min): 26679.D (-) m/ z 56.10 100.00% 56

5000 4 73 257 ' I ' ' ' ' I ' ' ' • I ’ ' 1 ' p • ' TI-T 1 101 129 29.20 29.40 29.60 29.80 30.00

m/z-> TTTTTTTTTTT 20 40 1187,11115,4 60 171185 i ' ' ' ■ i 80 100 120 140 160 180 200 220 240 260 280 300 213 239 ■ i ' ' ' ■ i ■ ' ■ ' i ■ | 11'1 11 1''1 11 1111 312 m/z 57. 47.10% Abundance #63261: 1-Hexene, 2-methyl- 56

41 5000 ■ i ■ • ' ■ i ■ ' ■ ■ i ■ 29.20 29.40 29.60 29.80 30.00 27 m/ Z 43.10 42.56% 70 98 / , ii ' I TTTII’EITTIUT ' I ' miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis( 1-methylethy)-, trans-

41 56 ...................... / ' I ' ' ' ' I ' 1 1 ' I AA+ 29.20 29.40 29.60 29.80 30.00 5000 m/ Z 41.10 39.57% 73 113128 TTTTTTTTTT TTTTT TEIE‘I‘‘‘11—1‘rT-"EII""IIT-EEII"TTIT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #25480: 2-Methyl-1 -tetradecene 56 29.20 29.40 29.60 29.80 30.00 m/z 55.10 32.41% 5000 -

70

m/z-> 27 42 I I |i, 9111125 154 182 210 ' ■ l ' • ■ ■ l ■ • ■ • । ■ • ■ > । t 1 • II . . . . । r. i . । i . 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 | . i i > | . . . . ।। . . . . । i . . i | i . . . । . . ■ . । . . > . । ___ AAA 29.20 29.40 29.60 29.80 30.00

26679.D NP112701.M Fri Dec 07 13:10:25 2001 Page 13

NYC-WTC_000032048

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NYC-WTC_000032048Source: NYC Law Department, mirrored locally

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