GCMS analysis comments for sample AD28694, Dec 2001

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Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28694.D Vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Oxirane, 2,3-bis(1-methylethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 29.43 4.13 ug/1 1020770 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H160 054644-32-5 32 2 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 3 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 25 4 Butyl hexadecanoate 312 C20H40O21 000000-00-0 25 Abundance 2. Scan 2657 (29.434 min): 28694.D (-) m/z 55.95 100.00% 53

5000 41 73 - — PP 129 257 239

mz-> I’ 20 m LA II 87 101 - 115 I 143157171 185199213 Hg 283. m 40 60 80 100 120 140 160 180 200 220 240 260 280 300 312 m/z 29.20 29.40 29.60 29.80 57.00 46.65% Abundance #5067: Oxirane, 2,3-bis(1-methylethyi)-, trans- 53 41

5000 1 ' i ■ A △ 29.20 29.40 29.60 29.80 TT

73 m/z 43.00 40.14% 113128 i• ■ ■ ■ i ■ i ’' ■' i'''' i' ''' i I ' ' ' 1 I 11 ' ‘ ‘ I i ■ ■ ■ ■ t m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354:1-Hexene, 2-methyl-

1 1 IT1 ■ ' 1 1 ■ 41 29.20 29.40 29.60 29.80 5000 m/z 41.00 39.06% 27 70 i' " 11'''' i'''' i'''' i'' ■ ■ r ■ ■' i' ’'11''' ■ i ■ ■ ■ ■ i' " ■ i ■' ■' i'''' i' " ' i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #28775: Pentadecane, 8-methylene- / ... — 29.20 29.40 29.60 29.80 m/z 55.00 30.54% 5000

27 70 84

m/z—> T‘‘t ’ I ° 20 40 60 98 12140....... 196—224................. 80 100 120 140 160 180 200 220 240 260 280 300 ...... AAA 29.20 29.40 29.60 29.80

28694.D GCMS1126.M Thu Dec 06 15:33:58 2001 Page 1

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